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机械化学法无溶剂无催化剂一锅合成吡喃并[2,3-d]嘧啶-2,4(1H,3H)-二酮,产率定量。

Mechanochemical solvent-free and catalyst-free one-pot synthesis of pyrano[2,3-d]pyrimidine-2,4(1H,3H)-diones with quantitative yields.

作者信息

Mashkouri Sara, Naimi-Jamal M Reza

机构信息

Organic Chemistry Research Laboratory, Department of Chemistry, Iran University of Science and Technology, 16846 Tehran, Iran.

出版信息

Molecules. 2009 Jan 19;14(1):474-9. doi: 10.3390/molecules14010474.

Abstract

Solvent-free synthesis of pyrano[2,3-d]pyrimidine-2,4(1H,3H)-diones by ball-milling and without any catalyst is described. This method provides several advantages such as being environmentally friendly, using a simple workup procedure, and affording high yields.

摘要

描述了通过球磨且无任何催化剂的方式无溶剂合成吡喃并[2,3-d]嘧啶-2,4(1H,3H)-二酮。该方法具有若干优点,如环境友好、后处理程序简单且产率高。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8bc2/6253776/f95d1746e348/molecules-14-00474-g001.jpg

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