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链状聚[[双-μ-碘代-二铜（I）（铜-铜）]双-（μ-4,4'-二-3-吡啶基-2,2'-二硫代二嘧啶）]

catena-Poly[[di-μ-iodido-dicopper(I)(Cu-Cu)]bis-(μ-4,4'-di-3-pyridyl-2,2'-disulfanediyldipyrimidine)].

作者信息

Zhu Hai-Bin

机构信息

School of Chemistry and Chemical Engineering, Southeast University, Nanjing 211189, People's Republic of China, and School of Material Science and Engineering, Southeast University, Nanjing 211189, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2009 Dec 12;66(Pt 1):m41. doi: 10.1107/S1600536809052325.

DOI:10.1107/S1600536809052325
PMID:21579940
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2980262/
Abstract

The title complex, Cu(2)I(2)(C(18)H(12)N(6)S(2))(2), contains a Cu(2)I(2) core with a Cu-Cu distance of 2.6935 (14) Å. The Cu(I) atom is coordinated by two bridging 4,4'-di-3-pyridyl-2,2'-disulfanediyldipyrimidine ligands and two bridging I atoms, forming a double chain.

摘要

标题配合物[Cu₂I₂(C₁₈H₁₂N₆S₂)₂]ₙ包含一个Cu₂I₂核心，铜-铜间距为2.6935(14) Å。Cu(I)原子由两个桥连的4,4'-二-3-吡啶基-2,2'-二硫代二嘧啶配体和两个桥连的碘原子配位，形成双链结构。

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本文引用的文献

1
4,4'-Di-3-pyridyl-2,2'-dithio-dipyrimidine.
Acta Crystallogr Sect E Struct Rep Online. 2009 May 14;65(Pt 6):o1253. doi: 10.1107/S1600536809016869.
2
A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.