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4,7-二苯基-2,9-双（三氯甲基）-1,10-菲咯啉

4,7-Diphenyl-2,9-bis-(trichloro-meth-yl)-1,10-phenanthroline.

作者信息

Xie Min-Hao, Liu Ya-Ling, Zou Pei, He Yong-Jun, Huang Biao

机构信息

Jiangsu Institute of Nuclear Medicine, Wuxi 214063, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2009 Dec 4;66(Pt 1):o5. doi: 10.1107/S1600536809051071.

DOI:10.1107/S1600536809051071
PMID:21580152
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2980224/
Abstract

In the title compound, C(26)H(14)Cl(6)N(2), the phenanthroline ring system is essentially planar, with an r.m.s. deviation of 0.048 (6) Å, and makes dihedral angles of 64.8 (14) and 66.6 (6)° with the two terminal phenyl rings. One of the trichloro-methyl groups is disordered over two positions, with occupancies of 0.42 (2) and 0.58 (2).

摘要

在标题化合物C(26)H(14)Cl(6)N(2)中，菲咯啉环系基本呈平面状，均方根偏差为0.048 (6) Å，与两个末端苯环的二面角分别为64.8 (14)°和66.6 (6)°。其中一个三氯甲基在两个位置上无序，占有率分别为0.42 (2)和0.58 (2)。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/dd04/2980224/aadf9a02b850/e-66-000o5-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/dd04/2980224/aadf9a02b850/e-66-000o5-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/dd04/2980224/aadf9a02b850/e-66-000o5-fig1.jpg

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