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N'-(2,4-二氯亚苄基)-4-甲氧基苯甲酰肼甲醇溶剂合物

N'-(2,4-Dichloro-benzyl-idene)-4-methoxy-benzohydrazide methanol solvate.

作者信息

Liang Min, Zou Dong-Hui

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2009 Jun 17;65(Pt 7):o1609. doi: 10.1107/S1600536809022624.

DOI:10.1107/S1600536809022624
PMID:21582882
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2969251/
Abstract

In the title compound, C(15)H(12)Cl(2)N(2)O(2)·CH(3)OH, the hydrazone mol-ecule displays an E configuration about the C=N bond. The dihedral angle between the two benzene rings is 4.6 (2)°. In the crystal structure, the hydrazone and methanol mol-ecules are linked into a chain propagating along the a axis via N-H⋯O and O-H⋯O hydrogen bonds.

摘要

在标题化合物C(15)H(12)Cl(2)N(2)O(2)·CH(3)OH中，腙分子围绕C=N键呈现E构型。两个苯环之间的二面角为4.6 (2)°。在晶体结构中，腙和甲醇分子通过N-H⋯O和O-H⋯O氢键连接成沿a轴延伸的链。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3698/2969251/a2c22d0d3404/e-65-o1609-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3698/2969251/193575d199fb/e-65-o1609-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3698/2969251/a2c22d0d3404/e-65-o1609-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3698/2969251/193575d199fb/e-65-o1609-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3698/2969251/a2c22d0d3404/e-65-o1609-fig2.jpg

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