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N'-(3,5-二氯-2-羟基亚苄基)-4-硝基苯甲酰肼甲醇溶剂合物

N'-(3,5-Dichloro-2-hy-droxy-benzyl-idene)-4-nitro-benzohydrazide methanol solvate.

作者信息

Zhu Hai-Yun

机构信息

Department of Chemistry and Chemical Engineering, Baoji University of Arts and Sciences, Baoji 721013, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2010 Sep 15;66(Pt 10):o2562. doi: 10.1107/S1600536810036184.

DOI:10.1107/S1600536810036184
PMID:21587548
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2983133/
Abstract

In the title compound, C(14)H(9)Cl(2)N(3)O(4)·CH(4)O, the dihedral angle between the two benzene rings in the hydrazone mol-ecule is 6.3 (3)°. An intra-molecular N-H⋯O hydrogen bond stabilizes the mol-ecular conformation. In the crystal, centrosymmetrically related mol-ecules are linked through inter-molecular O-H⋯O and N-H⋯O hydrogen bonds.

摘要

在标题化合物C₁₄H₉Cl₂N₃O₄·CH₄O中，腙分子中两个苯环之间的二面角为6.3 (3)°。分子内N—H⋯O氢键使分子构象稳定。在晶体中，中心对称相关的分子通过分子间O—H⋯O和N—H⋯O氢键相连。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1ab7/2983133/8c7182a22a99/e-66-o2562-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1ab7/2983133/8b9ff41e2d43/e-66-o2562-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1ab7/2983133/8c7182a22a99/e-66-o2562-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1ab7/2983133/8b9ff41e2d43/e-66-o2562-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1ab7/2983133/8c7182a22a99/e-66-o2562-fig2.jpg

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