N'-(3,5-二氯-2-羟基亚苄基)-4-硝基苯甲酰肼甲醇溶剂合物
N'-(3,5-Dichloro-2-hy-droxy-benzyl-idene)-4-nitro-benzohydrazide methanol solvate.
作者信息
Zhu Hai-Yun
机构信息
Department of Chemistry and Chemical Engineering, Baoji University of Arts and Sciences, Baoji 721013, People's Republic of China.
出版信息
Acta Crystallogr Sect E Struct Rep Online. 2010 Sep 15;66(Pt 10):o2562. doi: 10.1107/S1600536810036184.
Abstract
In the title compound, C(14)H(9)Cl(2)N(3)O(4)·CH(4)O, the dihedral angle between the two benzene rings in the hydrazone mol-ecule is 6.3 (3)°. An intra-molecular N-H⋯O hydrogen bond stabilizes the mol-ecular conformation. In the crystal, centrosymmetrically related mol-ecules are linked through inter-molecular O-H⋯O and N-H⋯O hydrogen bonds.
摘要
在标题化合物C₁₄H₉Cl₂N₃O₄·CH₄O中，腙分子中两个苯环之间的二面角为6.3 (3)°。分子内N—H⋯O氢键使分子构象稳定。在晶体中，中心对称相关的分子通过分子间O—H⋯O和N—H⋯O氢键相连。
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