Sensor Science Division,National Institute of Standards and Technology,Gaithersburg, Maryland 20899-8441,USA.
Software and Systems Division,National Institute of Standards and Technology,Boulder, Colorado 80305-3337,USA.
Microsc Microanal. 2019 Feb;25(1):70-76. doi: 10.1017/S1431927618016136.
Using a commercial X-ray tomography instrument, we have obtained reconstructions of a graded-index optical fiber with voxels of edge length 1.05 µm at 12 tube voltages. The fiber manufacturer created a graded index in the central region by varying the germanium concentration from a peak value in the center of the core to a very small value at the core-cladding boundary. Operating on 12 tube voltages, we show by a singular value decomposition that there are only two singular vectors with significant weight. Physically, this means scans beyond two tube voltages contain largely redundant information. We concentrate on an analysis of the images associated with these two singular vectors. The first singular vector is dominant and images of the coefficients of the first singular vector at each voxel look are similar to any of the single-energy reconstructions. Images of the coefficients of the second singular vector by itself appear to be noise. However, by averaging the reconstructed voxels in each of several narrow bands of radii, we can obtain values of the second singular vector at each radius. In the core region, where we expect the germanium doping to go from a peak value at the fiber center to zero at the core-cladding boundary, we find that a plot of the two coefficients of the singular vectors forms a line in the two-dimensional space consistent with the dopant decreasing linearly with radial distance from the core center. The coating, made of a polymer rather than silica, is not on this line indicating that the two-dimensional results are sensitive not only to the density but also to the elemental composition.
我们使用商用 X 射线断层成像仪器,在 12 个管电压下获得了具有 1.05μm 边长体素的梯度折射率光纤的重建。光纤制造商通过改变芯部中心的锗浓度,从峰值逐渐降低到芯-包边界的非常小值,在中心区域创建了梯度折射率。在 12 个管电压下工作,我们通过奇异值分解表明,只有两个奇异向量具有显著的权重。从物理意义上讲,这意味着超过两个管电压的扫描包含了大量冗余信息。我们专注于分析与这两个奇异向量相关的图像。第一个奇异向量占主导地位,并且在每个体素处的第一个奇异向量系数的图像看起来与任何单能重建都相似。第二个奇异向量本身的系数图像似乎是噪声。但是,通过在几个半径的窄带中对重建的体素进行平均,可以在每个半径处获得第二个奇异向量的系数值。在芯部区域,我们预计锗掺杂从光纤中心的峰值逐渐降低到芯-包边界的零值,我们发现奇异向量的两个系数的图在二维空间中形成一条线,与掺杂剂沿距芯中心的径向距离线性降低一致。聚合物制成的涂层而不是二氧化硅,不在这条线上,这表明二维结果不仅对密度敏感,而且对元素组成敏感。