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理解 PBF 工艺参数相互作用对 Ti-6Al-4V 表面性能的影响。

Understanding the effects of PBF process parameter interplay on Ti-6Al-4V surface properties.

机构信息

Department of Materials Science and Engineering, Monash University, Clayton, Victoria, Australia.

Monash Institute of Medical Engineering (MIME), Monash University, Clayton, Victoria, Australia.

出版信息

PLoS One. 2019 Aug 29;14(8):e0221198. doi: 10.1371/journal.pone.0221198. eCollection 2019.

Abstract

Ti-6Al-4V is commonly used in orthopaedic implants, and fabrication techniques such as Powder Bed Fusion (PBF) are becoming increasingly popular for the net-shape production of such implants, as PBF allows for complex customisation and minimal material wastage. Present research into PBF fabricated Ti-6Al-4V focuses on new design strategies (e.g. designing pores, struts or lattices) or mechanical property optimisation through process parameter control-however, it is pertinent to examine the effects of altering PBF process parameters on properties relating to bioactivity. Herein, changes in Ti-6Al-4V microstructure, mechanical properties and surface characteristics were examined as a result of varying PBF process parameters, with a view to understanding how to tune Ti-6Al-4V bio-activity during the fabrication stage itself. The interplay between various PBF laser scan speeds and laser powers influenced Ti-6Al-4V hardness, porosity, roughness and corrosion resistance, in a manner not clearly described by the commonly used volumetric energy density (VED) design variable. Key findings indicate that the relationships between PBF process parameters and ultimate Ti-6Al-4V properties are not straightforward as expected, and that wide ranges of porosity (0.03 ± 0.01% to 32.59 ± 2.72%) and corrosion resistance can be achieved through relatively minor changes in process parameters used-indicating volumetric energy density is a poor predictor of PBF Ti-6Al-4V properties. While variations in electrochemical behaviour with respect to the process parameters used in the PBF fabrication of Ti-6Al-4V have previously been reported, this study presents data regarding important surface characteristics over a large process window, reflecting the full capabilities of current PBF machinery.

摘要

钛-6 铝-4 钒通常用于矫形植入物,而粉末床融合(PBF)等制造技术正越来越多地用于此类植入物的净成型生产,因为 PBF 允许进行复杂的定制和最小的材料浪费。目前,对 PBF 制造的钛-6 铝-4 钒的研究集中在新的设计策略(例如设计孔、支柱或晶格)或通过工艺参数控制优化机械性能-然而,检查改变 PBF 工艺参数对与生物活性相关的性能的影响是很重要的。本文研究了由于改变 PBF 工艺参数而导致的钛-6 铝-4 钒微观结构、力学性能和表面特性的变化,以期了解如何在制造阶段本身调整钛-6 铝-4 钒的生物活性。各种 PBF 激光扫描速度和激光功率之间的相互作用影响了钛-6 铝-4 钒的硬度、孔隙率、粗糙度和耐腐蚀性,这种影响方式与常用的体积能量密度(VED)设计变量没有明确描述。主要发现表明,PBF 工艺参数与最终钛-6 铝-4 钒性能之间的关系并不像预期的那样直接,并且通过相对较小的工艺参数变化可以实现广泛的孔隙率(0.03±0.01%至 32.59±2.72%)和耐腐蚀性-这表明体积能量密度是 PBF 钛-6 铝-4 钒性能的一个较差的预测指标。虽然之前已经报道了 PBF 制造钛-6 铝-4 钒过程中工艺参数对电化学行为的变化,但本研究提供了关于大工艺窗口内重要表面特性的数据,反映了当前 PBF 机械的全部能力。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f8ec/6715245/48ab40ab8107/pone.0221198.g001.jpg

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