College of Material, Chemistry and Chemical Engineering, Hangzhou Normal University, Hangzhou 311121, China.
Org Biomol Chem. 2019 Dec 28;17(48):10201-10208. doi: 10.1039/c9ob02203a. Epub 2019 Nov 27.
An efficient protocol to synthesize 3-alkylated quinoxalin-2(1H)-ones through photocatalytic decarboxylation coupling reactions of quinoxalin-2(1H)-ones with N-hydroxyphthalimide ester was developed. The control experiment showed that a radical was involved in this transformation. This approach provides an alternative way to obtain various valuable corresponding products in moderate-to-good yields.
开发了一种通过光催化脱羧偶联反应将喹喔啉-2(1H)-酮与 N-羟基邻苯二甲酰亚胺酯合成 3-烷基化喹喔啉-2(1H)-酮的有效方法。控制实验表明，该转化涉及自由基。该方法为获得各种有价值的相应产物提供了一种替代方法，产率中等至良好。
