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从大猪毛菜果穗中提取新型天然纤维素纤维,用于环保型聚合物复合材料。

Characterization of a novel natural cellulosic fiber from Calotropis gigantea fruit bunch for ecofriendly polymer composites.

机构信息

Department of Mechanical Engineering, Kamaraj College of Engineering and Technology, Near Virudhunagar, Madurai District 625701, Tamilnadu, India.

Department of Mechatronics Engineering, Kamaraj College of Engineering and Technology, Near Virudhunagar, Madurai District 625701, Tamilnadu, India.

出版信息

Int J Biol Macromol. 2020 May 1;150:793-801. doi: 10.1016/j.ijbiomac.2020.02.134. Epub 2020 Feb 14.

Abstract

In this current research, the change in properties of alkali treatment on the physicochemical, structural, thermal and surface morphological properties of Calotropis gigantea fruit bunch (CGFB) fibers are investigated. The alkali-treatment was discovered to reduce the amorphous contents and removed the non-cellulosic components which were inveterate by the FTIR analysis. The X-ray diffraction pattern showed that the crystallinity index of the alkali-treated CGFB fibers was fairly higher than raw fibers. Thermal degradability and stability of alkali-treated Calotropis gigantea fruit bunch fibers were more than that of the untreated fiber. Scanning electron microscopy and Atomic force microscopy images showed the partially roughened surface of the fiber due to the removal of non-cellulosic elements and surface impurities during alkali treatment.

摘要

在本研究中,研究了碱处理对大猪毛菜果穗(CGFB)纤维的物理化学、结构、热和表面形貌特性的影响。通过傅里叶变换红外光谱(FTIR)分析发现,碱处理降低了无定形含量并去除了非纤维素成分。X 射线衍射图谱表明,碱处理后的 CGFB 纤维的结晶度指数明显高于原纤维。碱处理后的大猪毛菜果穗纤维的热降解性和热稳定性均优于未处理纤维。扫描电子显微镜和原子力显微镜图像显示,由于碱处理过程中非纤维素成分和表面杂质的去除,纤维表面呈现部分粗糙化。

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