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通过模压法制备的菜籽粕、果渣与微晶纤维素生物复合材料的性能:力学和物理化学特性

Properties of Biocomposites from Rapeseed Meal, Fruit Pomace and Microcrystalline Cellulose Made by Press Pressing: Mechanical and Physicochemical Characteristics.

作者信息

Żelaziński Tomasz

机构信息

Department of Production Engineering, Institute of Mechanical Engineering, Warsaw University of Life Sciences-SGGW, Nowoursynowska 164, 02-787 Warsaw, Poland.

出版信息

Materials (Basel). 2021 Feb 13;14(4):890. doi: 10.3390/ma14040890.

Abstract

This paper presents the results of research on biocomposites made of the mixture of post-extraction rapeseed meal, microcrystalline cellulose and various fruit pomace (chokeberry, blackcurrant, apple and raspberry pomace). The biocomposites were made in the process of mechanical thickening by means of a heated mould (die and stamp) which is located between two heating elements installed on a hydraulic press. The presented research combines mechanical engineering and material engineering issues. The physical and mechanical tests of obtained biocomposites included mechanical strength measurements, thermogravimetric analyses (TGA), colour change tests and scanning electron microscopic (SEM) tests of the internal structure after breaking the sample. In addition, Fourier transform infrared spectroscopy (FTIR) tests were carried out. Generally, the bend tests and Young's modulus were significantly increased, for example, biocomposites with an addition of chokeberry pomace had the flexural strength higher by approximately 25% in relation to the primary sample. Furthermore, it is interesting to note the increase of water contact angle of these biocomposites by 40% in relation to the primary sample. The research indicates the potential for using fruit pomace for the needs of biocomposite production.

摘要

本文介绍了由榨油后菜籽粕、微晶纤维素和各种果渣(黑果腺肋花楸果渣、黑加仑果渣、苹果果渣和树莓果渣)混合物制成的生物复合材料的研究结果。这些生物复合材料是通过机械增稠工艺,利用位于液压机上两个加热元件之间的加热模具(模具和压模)制成的。所呈现的研究结合了机械工程和材料工程问题。对所得生物复合材料进行的物理和力学测试包括机械强度测量、热重分析(TGA)、颜色变化测试以及样品断裂后内部结构的扫描电子显微镜(SEM)测试。此外,还进行了傅里叶变换红外光谱(FTIR)测试。一般来说,弯曲测试和杨氏模量显著提高,例如,添加黑果腺肋花楸果渣的生物复合材料的抗弯强度相对于原始样品提高了约25%。此外,值得注意的是,这些生物复合材料的水接触角相对于原始样品增加了40%。该研究表明了利用果渣满足生物复合材料生产需求的潜力。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/ee0e/7918066/e68b430e2a54/materials-14-00890-g001.jpg

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