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组合扫描高速原子力显微镜的误差分析。

Error Analysis of the Combined-Scan High-Speed Atomic Force Microscopy.

机构信息

College of Metrology and Measurement Engineering, China Jiliang University, Hangzhou 310018, China.

State Key Laboratory of Precision Measurement Technology and Instruments, Tianjin University, Tianjin 300072, China.

出版信息

Sensors (Basel). 2021 Sep 13;21(18):6139. doi: 10.3390/s21186139.

DOI:10.3390/s21186139
PMID:34577346
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC8471258/
Abstract

A combined tip-sample scanning architecture can improve the imaging speed of atomic force microscopy (AFM). However, the nonorthogonality between the three scanners and the nonideal response of each scanner cause measurement errors. In this article, the authors systematically analyze the influence of the installation and response errors of the combined scanning architecture. The experimental results show that when the probe in the homemade high-speed AFM moves with the Z-scanner, the spot position on the four-quadrant detector changes, thus introducing measurement error. Comparing the experimental results with the numerical and theoretical results shows that the undesired motion of the Z-scanner introduces a large error. The authors believe that this significant error occurs because the piezoelectric actuator not only stretches along the polarization direction but also swings under nonuniform multifield coupling. This article proposes a direction for further optimizing the instrument and provides design ideas for similar high-speed atomic force microscopes.

摘要

组合式针尖-样品扫描架构可以提高原子力显微镜(AFM)的成像速度。然而,三个扫描器之间的非正交性和每个扫描器的非理想响应会导致测量误差。在本文中,作者系统地分析了组合扫描架构的安装和响应误差的影响。实验结果表明,当自制高速 AFM 中的探针随 Z 扫描器移动时,四象限探测器上的光斑位置会发生变化,从而引入测量误差。将实验结果与数值和理论结果进行比较表明,Z 扫描器的非预期运动引入了较大的误差。作者认为,这种显著的误差是由于压电致动器不仅沿极化方向伸缩,而且在非均匀多场耦合下摆动所致。本文为进一步优化仪器提出了方向,并为类似的高速原子力显微镜提供了设计思路。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2ec2/8471258/2539f7ce3ea0/sensors-21-06139-g011.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2ec2/8471258/2fa40ccd543d/sensors-21-06139-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2ec2/8471258/8fcc3d42e26a/sensors-21-06139-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2ec2/8471258/cd090781b355/sensors-21-06139-g003.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2ec2/8471258/bf239f6ea51c/sensors-21-06139-g004.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2ec2/8471258/b2a456df516b/sensors-21-06139-g005.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2ec2/8471258/598296c9b178/sensors-21-06139-g006.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2ec2/8471258/8bb835eb6088/sensors-21-06139-g007.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2ec2/8471258/196a8c44d5b1/sensors-21-06139-g008.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2ec2/8471258/c1d1772fed33/sensors-21-06139-g009.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2ec2/8471258/3df8c2c7216a/sensors-21-06139-g010.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2ec2/8471258/2539f7ce3ea0/sensors-21-06139-g011.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2ec2/8471258/2fa40ccd543d/sensors-21-06139-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2ec2/8471258/8fcc3d42e26a/sensors-21-06139-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2ec2/8471258/cd090781b355/sensors-21-06139-g003.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2ec2/8471258/bf239f6ea51c/sensors-21-06139-g004.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2ec2/8471258/b2a456df516b/sensors-21-06139-g005.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2ec2/8471258/598296c9b178/sensors-21-06139-g006.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2ec2/8471258/8bb835eb6088/sensors-21-06139-g007.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2ec2/8471258/196a8c44d5b1/sensors-21-06139-g008.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2ec2/8471258/c1d1772fed33/sensors-21-06139-g009.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2ec2/8471258/3df8c2c7216a/sensors-21-06139-g010.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2ec2/8471258/2539f7ce3ea0/sensors-21-06139-g011.jpg

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本文引用的文献

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ACS Nano. 2021 Feb 23;15(2):2229-2239. doi: 10.1021/acsnano.0c06820. Epub 2020 Dec 10.
2
Development of electrochemical high-speed atomic force microscopy for visualizing dynamic processes of battery electrode materials.用于可视化电池电极材料动态过程的电化学高速原子力显微镜的发展。
Rev Sci Instrum. 2020 Oct 1;91(10):103701. doi: 10.1063/5.0024425.
3
Atomic force microscopy-based single-molecule force spectroscopy detects DNA base mismatches.
原子力显微镜的单分子力谱检测 DNA 碱基错配。
Nanoscale. 2019 Oct 7;11(37):17206-17210. doi: 10.1039/c9nr05234h. Epub 2019 Sep 17.
4
High-speed atomic force microscope with a combined tip-sample scanning architecture.具有组合式针尖-样品扫描结构的高速原子力显微镜。
Rev Sci Instrum. 2019 Jun;90(6):063707. doi: 10.1063/1.5089534.
5
Adaptive velocity-dependent proportional-integral controller for high-speed atomic force microscopy.用于高速原子力显微镜的自适应速度相关比例积分控制器。
J Microsc. 2019 Aug;275(2):107-114. doi: 10.1111/jmi.12819. Epub 2019 Jun 10.
6
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Functional extension of high-speed AFM for wider biological applications.高速原子力显微镜在更广泛生物应用中的功能扩展。
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Method of mechanical holding of cantilever chip for tip-scan high-speed atomic force microscope.用于针尖扫描高速原子力显微镜的悬臂芯片机械固定方法。
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Advances in lead-free piezoelectric materials for sensors and actuators.无铅压电材料在传感器和执行器中的研究进展。
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