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基于射频磁控溅射法沉积的ZnO薄膜的高分辨率声学传感器的研制。

Development of a High-Resolution Acoustic Sensor Based on ZnO Film Deposited by the RF Magnetron Sputtering Method.

作者信息

Kang Dong-Chan, Kim Jeong-Nyeon, Park Ik-Keun

机构信息

Graduate School of Nano IT Design Fusion, Seoul National University of Science and Technology, 232, Gongneung-ro, Nowon-gu, Seoul 01811, Korea.

Ginzton Laboratory, Stanford University, Stanford, CA 94305, USA.

出版信息

Materials (Basel). 2021 Nov 14;14(22):6870. doi: 10.3390/ma14226870.

Abstract

In the study, an acoustic sensor for a high-resolution acoustic microscope was fabricated using zinc oxide (ZnO) piezoelectric ceramics. The c-cut sapphire was processed into a lens shape to deposit a ZnO film using radio frequency (RF) magnetron sputtering, and an upper and a lower electrode were deposited using E-beam evaporation. The electrode was a Au thin film, and a Ti thin film was used as an adhesion layer. The surface microstructure of the ZnO film was observed using a scanning electron microscope (SEM), the thickness of the film was measured using a focused ion beam (FIB) for piezoelectric ceramics deposited on the sapphire wafer, and the thickness of ZnO was measured to be 4.87 μm. As a result of analyzing the crystal growth plane using X-ray diffraction (XRD) analysis, it was confirmed that the piezoelectric characteristics were grown to the (0002) plane. The sensor fabricated in this study had a center frequency of 352 MHz. The bandwidth indicates the range of upper (375 MHz) and lower (328 MHz) frequencies at the -6 dB level of the center frequency. As a result of image analysis using the resolution chart, the resolution was about 1 μm.

摘要

在该研究中,使用氧化锌(ZnO)压电陶瓷制造了一种用于高分辨率声学显微镜的声学传感器。将c切割蓝宝石加工成透镜形状,以便使用射频(RF)磁控溅射沉积ZnO薄膜,并使用电子束蒸发沉积上下电极。电极是金薄膜,钛薄膜用作粘附层。使用扫描电子显微镜(SEM)观察ZnO薄膜的表面微观结构,对于沉积在蓝宝石晶片上的压电陶瓷,使用聚焦离子束(FIB)测量薄膜的厚度,测得ZnO的厚度为4.87μm。通过X射线衍射(XRD)分析晶体生长平面的结果表明,压电特性沿(0002)平面生长。本研究中制造的传感器中心频率为352 MHz。带宽表示中心频率-6 dB水平下的上限频率(375 MHz)和下限频率(328 MHz)范围。使用分辨率测试图进行图像分析的结果表明,分辨率约为1μm。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9e19/8624261/9b1456535859/materials-14-06870-g001.jpg

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