Qin Hui-Wei, Yang Tian-Mei, Yang Shao-Bing, Yang Mei-Quan, Wang Yuan-Zhong, Zhang Jin-Yu
Medicinal Plants Research Institute, Yunnan Academy of Agricultural Sciences, Kunming, China.
College of Traditional Chinese Medicine, Yunnan University of Chinese Medicine, Kunming, China.
Front Plant Sci. 2022 Feb 25;13:803776. doi: 10.3389/fpls.2022.803776. eCollection 2022.
The effects of twelve different pre-drying and drying methods on the chemical composition in the pericarp and kernel of were studied. The volatile components were isolated from the samples by simultaneous distillation and extraction and analyzed by gas chromatography-mass spectrometry (GC-MS). Sixty and thirty-eight compounds were identified from pericarp and kernel, respectively, and the main constituents were oxygenated monoterpenes. These compounds were not only significantly affected by pre-drying and drying methods but also varied in content due to different tissue locations. The total volatile content of pericarp varied from 0.70 to 1.55%, with the highest obtained by microwave-dried samples (150 W) and the lowest in freeze-dried samples. The total volatile content of the kernel varied from 6.11 to 10.69%, with the highest content obtained during sun drying (SD) and the lowest content in samples treated with boiling water for 2 min. Oxygenated monoterpenes were the highest compounds in pericarp and kernel, which were also the most affected by drying methods. The highest content of oxygenated monoterpenes in the pericarp (0.77%) could be obtained by boiling water treatment for 5 min, and the highest content of oxygenated monoterpenes in the kernel (7.48%) could be obtained by SD. Additionally, the main components such as 1,8-cineole, 2-carene, ()-citral, nerolidol, ()-2-decenal, ()-2-dodecenal, citral, ()-2-octenal, 4-propylbenzaldehyde, and phthalan showed remarkable variations in pre-drying and drying methods.
研究了12种不同的预干燥和干燥方法对[具体研究对象]果皮和果仁化学成分的影响。采用同时蒸馏萃取法从样品中分离挥发性成分,并通过气相色谱-质谱联用仪(GC-MS)进行分析。分别从果皮和果仁中鉴定出60种和38种化合物,主要成分是氧化单萜。这些化合物不仅受到预干燥和干燥方法的显著影响,而且由于组织位置不同,其含量也有所变化。果皮的总挥发物含量在0.70%至1.55%之间,其中微波干燥样品(150W)的含量最高,冷冻干燥样品的含量最低。果仁的总挥发物含量在6.11%至10.69%之间,其中日晒干燥(SD)时含量最高,用沸水处理2分钟的样品含量最低。氧化单萜是果皮和果仁中含量最高的化合物,也是受干燥方法影响最大的化合物。果皮中氧化单萜的最高含量(0.77%)可通过沸水处理5分钟获得,果仁中氧化单萜的最高含量(7.48%)可通过日晒干燥获得。此外,1,8-桉叶素、2-蒈烯、()-柠檬醛、橙花叔醇、()-2-癸烯醛、()-2-十二碳烯醛、柠檬醛、()-2-辛烯醛、4-丙基苯甲醛和酞嗪等主要成分在预干燥和干燥方法上表现出显著差异。