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采用亚临界二甲醚法从湿南极磷虾中提取油脂。

Extraction of oil from wet Antarctic krill () using a subcritical dimethyl ether method.

作者信息

Liu Shulai, Hu Wei, Fang Yizhou, Cai Yanping, Zhang Jianyou, Liu Jianhua, Ding Yuting

机构信息

Department of Food Science and Engineering, Ocean College, Zhejiang University of Technology Hangzhou 310014 P. R. China

National R & D Branch Center for Pelagic Aquatic Products Processing (Hangzhou) Hangzhou 310014 P. R. China.

出版信息

RSC Adv. 2019 Oct 24;9(59):34274-34282. doi: 10.1039/c9ra06238f. eCollection 2019 Oct 23.

Abstract

In this study, a novel method for obtaining high-quality krill oil from wet Antarctic krill by using subcritical dimethyl ether (SDE) was proposed. A response surface design was used to obtain the best SDE extraction parameters. The optimum extraction efficiency of 93.77 ± 0.92% was obtained at a stirring speed of 1030 rpm, temperature of 47 °C and dynamic extraction time of 90 min. Compared with -hexane, ethanol, supercritical CO and subcritical -butane extraction, the krill oil extracted by SDE exhibited low peroxide values (1.46 ± 0.26 mmol kg), high astaxanthin (218.06 ± 4.74 mg kg), phosphatidylcholine (PC) (33.95 ± 0.65%), and phosphatidylethanolamine (PE) (11.67 ± 0.23%) content. Moreover, krill oil extracted by SDE has high levels of EPA (16.38 ± 0.05%) and DHA (7.91 ± 0.07%). SDE extraction proved to be an efficient and safe method for extraction of quality krill oil from wet Antarctic krill, and it could be a promising method for oil extraction in wet food in future.

摘要

本研究提出了一种利用亚临界二甲醚(SDE)从湿南极磷虾中获取高品质磷虾油的新方法。采用响应面设计来获得最佳的SDE提取参数。在搅拌速度为1030转/分钟、温度为47℃和动态提取时间为90分钟的条件下,获得了93.77±0.92%的最佳提取效率。与己烷、乙醇、超临界CO₂和亚临界丁烷提取相比,SDE提取的磷虾油具有较低的过氧化值(1.46±0.26毫摩尔/千克)、较高的虾青素(218.06±4.74毫克/千克)、磷脂酰胆碱(PC)(33.95±0.65%)和磷脂酰乙醇胺(PE)(11.67±0.23%)含量。此外,SDE提取的磷虾油中二十碳五烯酸(EPA)(16.38±0.05%)和二十二碳六烯酸(DHA)(7.91±0.07%)含量较高。SDE提取被证明是一种从湿南极磷虾中提取优质磷虾油的高效且安全的方法,并且可能成为未来湿食品中油脂提取的一种有前景的方法。

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