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通过新型绿色方法制备的银纳米结构作为生物和环境应用的有效平台。

Silver nanostructures prepared via novel green approach as an effective platform for biological and environmental applications.

作者信息

Rani Pooja, Ahmed Bilal, Singh Jagpreet, Kaur Jasmeen, Rawat Mohit, Kaur Navjot, Matharu Avtar Singh, AlKahtani Muneera, Alhomaidi Eman A H, Lee Jintae

机构信息

Department of Nanotechnology, Sri Guru Granth Sahib World University, Fatehgarh Sahib 140406, Punjab, India.

School of Chemical Engineering, Yeungnam University, Republic of Korea.

出版信息

Saudi J Biol Sci. 2022 Jun;29(6):103296. doi: 10.1016/j.sjbs.2022.103296. Epub 2022 Apr 22.

Abstract

Silver nanoparticles play a significant role in biomedical sciences due to their unique properties allowing for their use as an effective sensing and remediation platform Herein, the green synthesis of silver nanostructures (Ag NSs), prepared via aqueous extract of waste leaves in the presence of silver nitrate solution (10 M), is reported. The Ag NSs are fully characterized and their efficacy with respect to 4-nitrophenol reduction, glucose sensing, and microbes is determined. Visually, the color of silver nitrate containing solution altered from colorless to yellowish, then reddish grey, confirming the formation of Ag NSs. HRTEM and SEAD studies revealed the Ag NSs to have different morphologies (triangular, rod-shaped, hexagonal, within a size range of 20-40 nm) with face-centered cubic ( crystal structure. The Ag NSs possess high efficacy for nitrophenol reduction (<11 min and degradation efficiency of 98.2%), glucose sensing (LOD: 5.83 µM), and antimicrobial activity ( with clearance zones of 18.3 and 14 mm, respectively). Thus, the current study alludes towards the development of a cost-effective, sustainable, and efficient three-in-one platform for biomedical and environmental applications.

摘要

由于其独特的性质,银纳米颗粒在生物医学科学中发挥着重要作用,使其能够用作有效的传感和修复平台。在此,报道了通过废叶水提取物在硝酸银溶液(10 M)存在下制备银纳米结构(Ag NSs)的绿色合成方法。对Ag NSs进行了全面表征,并测定了其在4-硝基苯酚还原、葡萄糖传感和微生物方面的功效。从视觉上看,含硝酸银溶液的颜色从无色变为淡黄色,然后变为红灰色,证实了Ag NSs的形成。高分辨率透射电子显微镜(HRTEM)和选区电子衍射(SEAD)研究表明,Ag NSs具有不同的形态(三角形、棒状、六边形),尺寸范围为20-40纳米,具有面心立方晶体结构。Ag NSs在硝基苯酚还原方面具有高效性(<11分钟,降解效率为98.2%)、葡萄糖传感(检测限:5.83 μM)和抗菌活性(清除区分别为18.3和14毫米)。因此,当前的研究暗示了一种用于生物医学和环境应用的经济高效、可持续的三合一平台的开发。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3125/9092993/b856e7c0d1b6/ga1.jpg

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