Klaisiri Awiruth, Phumpatrakom Panupat, Thamrongananskul Niyom
Division of Restorative Dentistry, Faculty of Dentistry, Thammasat University, Pathum Thani, Thailand.
Division of Endodontics, Faculty of Dentistry, Thammasat University, Pathum Thani, Thailand.
Eur J Dent. 2023 Jul;17(3):804-808. doi: 10.1055/s-0042-1755627. Epub 2022 Oct 11.
This study examined the chemical surface modification methods of resin composite repaired with resin-modified glass-ionomer cement (RMGIC).
Ninety aged resin composite rods were produced and sorted into 9 groups of 10 specimens and surface modified with silane agent and/or bonding agent as follows: group 1, no surface modified; group 2, etch + single bond 2 (SB2); group 3, SB2; group 4, etch + RelyX ceramic primer (RXP) + SB2; group 5, RXP + SB2; group 6, etch + single bond universal (SU); group 7, SU; group 8, etch + RXP + SU; and group 9, RXP + SU. A clear silicone mold was placed on the top of specimen center, and then filled with RMGIC. The specimens' shear bond strengths (SBSs) were examined in mechanical testing equipment. To determine failure types, the fractured specimen surfaces were inspected using a stereomicroscope.
The data collected were analyzed using one-way analysis of variance, and significance level was operated using Tukey's test ( < 0.05).
Group 8 had the greatest SBS, but it was statistically indistinguishable from groups 4, 5, and 9. The most frequent fracture mode was adhesive failure. High SBS was commonly associated with mixed failure.
The use of bonding agents enhances the resin composite's wettability and allows it to bond to RMGIC. Moreover, the use of the silane coupling agent before applying bonding agent showed significantly higher bonding ability of resin composite and RMGIC interface.
本研究探讨了用树脂改性玻璃离子水门汀(RMGIC)修复树脂复合材料的化学表面改性方法。
制备90根老化的树脂复合棒,分为9组,每组10个样本,并按如下方式用硅烷剂和/或粘结剂进行表面改性:第1组,未进行表面改性;第2组,蚀刻+单键2(SB2);第3组,SB2;第4组,蚀刻+RelyX陶瓷底漆(RXP)+SB2;第5组,RXP+SB2;第6组,蚀刻+单键通用型(SU);第7组,SU;第8组,蚀刻+RXP+SU;第9组,RXP+SU。在样本中心顶部放置一个透明硅胶模具,然后注入RMGIC。在机械测试设备中检测样本的剪切粘结强度(SBS)。为确定失效类型,使用体视显微镜检查断裂样本的表面。
收集的数据采用单因素方差分析进行分析,显著性水平采用Tukey检验(<0.05)。
第8组的SBS最大,但与第4、5和9组在统计学上无显著差异。最常见的断裂模式是粘结失效。高SBS通常与混合失效相关。
使用粘结剂可提高树脂复合材料的润湿性,并使其与RMGIC粘结。此外,在应用粘结剂之前使用硅烷偶联剂可显著提高树脂复合材料与RMGIC界面的粘结能力。