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优化超声辅助提取工艺以从西瓜皮中获取总酚类和黄酮类化合物。

Optimization of the ultrasonic-assisted extraction process to obtain total phenolic and flavonoid compounds from watermelon ( rind.

作者信息

Vo Tan Phat, Nguyen Le Ngoc Huong, Le Nguyen Phuc Thien, Mai Thanh Phong, Nguyen Dinh Quan

机构信息

Laboratory of Biofuel and Biomass Research, Faculty of Chemical Engineering, Ho Chi Minh University of Technology (HCMUT), 268 Ly Thuong Kiet Street, District 10, Ho Chi Minh City, Viet Nam.

Vietnam National University Ho Chi Minh City, Linh Trung Ward, Thu Duc City, Ho Chi Minh City, Viet Nam.

出版信息

Curr Res Food Sci. 2022 Sep 20;5:2013-2021. doi: 10.1016/j.crfs.2022.09.021. eCollection 2022.

DOI:10.1016/j.crfs.2022.09.021
PMID:36337913
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC9626904/
Abstract

This context presents the study of ultrasonic-assisted extraction (UAE) to obtain phenolic and flavonoid compounds from watermelon rind powder (WRP). The antioxidant activity of the extracts was investigated using DPPH and ABTS assays. One-factor experiments were conducted to examine the effect of each factor (solid-to-liquid ratio (SLR), acetone concentration (AC), temperature, and time) on the UAE of WRP. Box-Behnken Design (BDD) model was employed to optimize the UAE conditions based on total phenolic contents (TPC), total flavonoid content (TFC), and their antioxidant activities. The optimal conditions were 1:30.50 SLR, 70.71% AC, 29.78 °C, and 10.65 min extraction time. There were no significant differences between predicted and experimental results (less than 6.0%), recommending a feasible and innovative process of deploying UAE to extract phenolics and flavonoids effectively from watermelon rind.

摘要

本文介绍了采用超声辅助提取（UAE）从西瓜皮粉（WRP）中获取酚类和黄酮类化合物的研究。使用DPPH和ABTS分析法研究了提取物的抗氧化活性。进行单因素实验以考察各因素（固液比（SLR）、丙酮浓度（AC）、温度和时间）对WRP超声辅助提取的影响。采用Box-Behnken设计（BDD）模型，基于总酚含量（TPC）、总黄酮含量（TFC）及其抗氧化活性对超声辅助提取条件进行优化。最佳条件为固液比1:30.50、丙酮浓度70.71%、温度29.78℃、提取时间10.65分钟。预测结果与实验结果之间无显著差异（小于6.0%），表明采用超声辅助提取从西瓜皮中有效提取酚类和黄酮类化合物是一种可行且创新的工艺。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f76c/9626904/4355bf1373df/gr6.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f76c/9626904/959271104c8a/ga1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f76c/9626904/82aa7addfe20/gr1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f76c/9626904/b55c4596ccc4/gr2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f76c/9626904/5acb04847fbd/gr3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f76c/9626904/b0416f4a73df/gr4.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f76c/9626904/cc02ddceb30b/gr5.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f76c/9626904/4355bf1373df/gr6.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f76c/9626904/959271104c8a/ga1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f76c/9626904/82aa7addfe20/gr1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f76c/9626904/b55c4596ccc4/gr2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f76c/9626904/5acb04847fbd/gr3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f76c/9626904/b0416f4a73df/gr4.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f76c/9626904/cc02ddceb30b/gr5.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f76c/9626904/4355bf1373df/gr6.jpg

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