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正畸粘结剂的力学性能及其在酸性环境中的行为

Mechanical Properties of Orthodontic Cements and Their Behavior in Acidic Environments.

作者信息

Iosif Cristina, Cuc Stanca, Prodan Doina, Moldovan Marioara, Petean Ioan, Labunet Anca, Barbu Tudoran Lucian, Badea Iulia Clara, Man Sorin Claudiu, Badea Mîndra Eugenia, Chifor Radu

机构信息

Department of Prosthetic Dentistry and Dental Materials, "Iuliu Hatieganu" University of Medicine and Pharmacy, 32 Clinicilor Street, 400006 Cluj-Napoca, Romania.

Department of Polymer Composites, Institute of Chemistry "Raluca Ripan", University Babes-Bolyai, 30 Fantanele Street, 400294 Cluj-Napoca, Romania.

出版信息

Materials (Basel). 2022 Nov 9;15(22):7904. doi: 10.3390/ma15227904.

Abstract

The present research is focused on three different classes of orthodontic cements: resin composites (e.g., BracePaste); resin-modified glass ionomer RMGIC (e.g., Fuji Ortho) and resin cement (e.g., Transbond). Their mechanical properties such as compressive strength, diametral tensile strength and flexural strength were correlated with the samples' microstructures, liquid absorption, and solubility in liquid. The results show that the best compressive (100 MPa) and flexural strength (75 Mpa) was obtained by BracePaste and the best diametral tensile strength was obtained by Transbond (230 MPa). The lowestvalues were obtained by Fuji Ortho RMGIC. The elastic modulus is relatively high around 14 GPa for BracePaste, and Fuji Ortho and Transbond have only 7 GPa. The samples were also subjected to artificial saliva and tested in different acidic environments such as Coca-Cola and Red Bull. Their absorption and solubility were investigated at different times ranging from 1 day to 21 days. Fuji Ortho presents the highest liquid absorption followed by Transbond, the artificial saliva has the best absorption and Red Bull has the lowest absorption. The best resistance to the liquids was obtained by BracePaste in all environments. Coca-Cola presents values four times greater than the ones observed for artificial saliva. Solubility tests show that BracePaste is more soluble in artificial saliva, and Fuji Ortho and Transbond are more soluble in Red Bull and Coca-Cola. Scanning electron microscopy (SEM) images evidenced a compact structure for BracePaste in all environments sustaining the lower liquid absorption values. Fuji Ortho and Transbond present a fissure network allowing the liquid to carry out in-depth penetration of materials. SEM observations are in good agreement with the atomic force microscopy (AFM) results. The surface roughness decreases with the acidity increasing for BracePaste meanwhile it increases with the acidity for Fuji Ortho and Transbond. In conclusion: BracePaste is recommended for long-term orthodontic treatment for patients who regularly consume acidic beverages, Fuji Ortho is recommended for short-term orthodontic treatment for patients who regularly consume acidic beverages and Transbond is recommended for orthodontic treatment over an average time period for patients who do not regularly consume acidic beverages.

摘要

本研究聚焦于三类不同的正畸用粘结剂

树脂复合材料(如BracePaste);树脂改性玻璃离子水门汀(RMGIC,如Fuji Ortho)和树脂粘结剂(如Transbond)。它们的力学性能,如抗压强度、径向拉伸强度和弯曲强度,与样品的微观结构、吸液率及在液体中的溶解度相关。结果表明,BracePaste的抗压强度(100MPa)和弯曲强度(75MPa)最佳,Transbond的径向拉伸强度最佳(230MPa)。Fuji Ortho RMGIC的各项强度值最低。BracePaste的弹性模量相对较高,约为14GPa,而Fuji Ortho和Transbond仅为7GPa。样品还被置于人工唾液中,并在不同酸性环境(如可口可乐和红牛饮料)中进行测试。研究了它们在1天至21天不同时间的吸液率和溶解度。Fuji Ortho的吸液率最高,其次是Transbond,人工唾液的吸液率最佳,红牛饮料的吸液率最低。在所有环境中,BracePaste对液体的耐受性最佳。可口可乐中的各项数值比人工唾液中的数值大四倍。溶解度测试表明,BracePaste在人工唾液中更易溶解,而Fuji Ortho和Transbond在红牛饮料和可口可乐中更易溶解。扫描电子显微镜(SEM)图像显示,在所有环境中BracePaste都具有致密结构,这使其吸液率较低。Fuji Ortho和Transbond呈现出裂隙网络,使液体能够深入渗透材料。SEM观察结果与原子力显微镜(AFM)结果高度吻合。对于BracePaste,表面粗糙度随酸度增加而降低,而对于Fuji Ortho和Transbond,表面粗糙度随酸度增加而增加。总之:对于经常饮用酸性饮料的患者,推荐使用BracePaste进行长期正畸治疗;对于经常饮用酸性饮料的患者,推荐使用Fuji Ortho进行短期正畸治疗;对于不经常饮用酸性饮料的患者,推荐使用Transbond进行平均时长的正畸治疗。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b5ff/9697370/1f2b73d2cce3/materials-15-07904-g001.jpg

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