College of Traffic Engineering, Nanjing Vocational University of Industry Technology, Nanjing, China.
PLoS One. 2023 Mar 27;18(3):e0283456. doi: 10.1371/journal.pone.0283456. eCollection 2023.
The research aims to study the application of remote Femto Second (FS) technology in black silicon material preparation and optical devices. Based on the principle and characteristic research of FS technology, the interaction between FS and silicon is adopted to propose a scheme for preparing black silicon material through experiments. Moreover, the experimental parameters are optimized. Then, the scheme of using the FS for etching polymer optical power splitter as a new technical means is proposed. In addition, while ensuring processing accuracy, the appropriate process parameters of laser etching photoresist are obtained. The results show that the performance of black silicon prepared with SF6 as the background gas is greatly improved in the 400-2200nm range. However, the performance of black silicon samples with the two-layer structure etched at different laser energy densities has little difference. Black silicon with a Se+Si two-layer film structure has the best optical absorption performance in the infrared range of 1100nm-2200nm. Besides, the optical absorption rate is the highest when the laser scanning rate is 0.5mm/s. In the band of >1100nm, when the maximum laser energy density is 6.5kJ/m2, the overall absorption of the etched sample is the worst. The absorption rate is the best when the laser energy density is 3.9kJ/m2. It suggests that the proper parameter selection greatly impacts the quality of the final laser-etched sample.
这项研究旨在探讨远程飞秒(FS)技术在黑硅材料制备和光学器件中的应用。基于 FS 技术的原理和特性研究,采用 FS 与硅的相互作用,提出了通过实验制备黑硅材料的方案,并对实验参数进行了优化。然后,提出了利用 FS 作为新的技术手段来刻蚀聚合物光功率分束器的方案。此外,在保证加工精度的同时,获得了适当的激光刻蚀光刻胶的工艺参数。结果表明,以 SF6 为背景气体制备的黑硅在 400-2200nm 范围内的性能得到了很大的提高。然而,不同激光能量密度下刻蚀的双层结构黑硅样品的性能差异不大。具有 Se+Si 双层膜结构的黑硅在 1100nm-2200nm 红外波段具有最佳的光学吸收性能,并且当激光扫描速率为 0.5mm/s 时,光学吸收率最高。在>1100nm 波段,当最大激光能量密度为 6.5kJ/m2 时,刻蚀样品的整体吸收率最差。当激光能量密度为 3.9kJ/m2 时,吸收率最佳。这表明适当的参数选择对最终激光刻蚀样品的质量有很大的影响。