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评价纳米氧化石墨烯对传统型和树脂改性型玻璃离子水门汀剪切粘结强度的影响。

Evaluation of the effect of nano-graphene oxide on shear bond strength of conventional and resin-modified glass ionomer cement.

机构信息

Department of Operative Dentistry, Biomaterials Research Center, School of Dentistry, Shiraz University of Medical Sciences, Shiraz, Iran.

Department of Operative Dentistry, School of Dentistry, Shiraz University of Medical Sciences, Shiraz, Iran.

出版信息

Clin Exp Dent Res. 2023 Oct;9(5):851-858. doi: 10.1002/cre2.789. Epub 2023 Sep 22.

Abstract

OBJECTIVES

Recently, nano-graphene oxide (nGO), a material with unique mechanical properties, has been introduced to improve the properties of glass ionomer cement (GIC). The purpose of this study was to investigate the effect of adding nGO on the shear bond strength (SBS) of conventional (CGIC) and resin-modified GIC (RMGIC).

METHODS

Sixty intact molars were mounted and their occlusal surface was cut at a depth of 1 mm below the dentinoenamel junction. 1 wt.% and 2 wt.% of nGO (US Research Nanomaterials, Inc.) were added to CGIC and RMGIC (GC Corporation). The samples were randomly divided into six groups (n = 10), including 1: CGIC,  2: CGIC + 1% GO, 3: CGIC + 2% GO, 4: RMGIC, 5: RMGIC + 1% GO, and 6: RMGIC + 2% GO. Plastic molds were placed on the surface of the dentin pretreated with 10% polyacrylic acid (GC Corporation) and filled with prepared cement according to the manufacturer's instruction. After 24 h of storage in an incubator, the SBS test was done by the universal testing machine. Data were analyzed using two-way analysis of variance and post hoc Tukey tests (p < .05).

RESULTS

In the group of CGIC, mean SBS was significantly lower than all other study groups (p < .001), and groups 5 (RMGIC + 1% GO) and 6 (RMGIC + 2% GO) showed significantly higher values compared to all other study groups (p < .001). However, the difference between groups 2 and 3, as well as the difference between groups 5 and 6, was not significant (p = .999 andp = .994, respectively). RMGI groups had significantly higher SBS than their corresponding CGIC groups.

CONCLUSIONS

The addition of 1% and 2% nGO significantly increased the SBS of CGIC and RMGIC to the dentin, which can be considered as a promising point for wider clinical application of this material.

摘要

目的

最近,具有独特机械性能的纳米氧化石墨烯(nGO)已被引入以改善玻璃离子水门汀(GIC)的性能。本研究的目的是研究添加 nGO 对传统(CGIC)和树脂改性 GIC(RMGIC)剪切粘结强度(SBS)的影响。

方法

将 60 颗完整的磨牙固定,在牙本质牙釉质交界处下方 1mm 处切割其咬合面。将 1wt.%和 2wt.%的 nGO(美国研究纳米材料公司)添加到 CGIC 和 RMGIC(GC 公司)中。将样本随机分为六组(n=10),包括 1:CGIC,2:CGIC+1%GO,3:CGIC+2%GO,4:RMGIC,5:RMGIC+1%GO,和 6:RMGIC+2%GO。将预处理过的牙本质表面放置塑料模具,用 10%聚丙烯酸(GC 公司)处理,根据制造商的说明填充准备好的水泥。在孵育箱中储存 24 小时后,通过万能试验机进行 SBS 测试。使用双因素方差分析和事后 Tukey 检验(p<0.05)对数据进行分析。

结果

在 CGIC 组中,平均 SBS 明显低于所有其他研究组(p<0.001),而第 5 组(RMGIC+1%GO)和第 6 组(RMGIC+2%GO)与所有其他研究组相比,显示出明显更高的值(p<0.001)。然而,第 2 组和第 3 组之间的差异以及第 5 组和第 6 组之间的差异不显著(p=0.999 和 p=0.994)。RMGI 组的 SBS 明显高于其相应的 CGIC 组。

结论

添加 1%和 2%的 nGO 可显著提高 CGIC 和 RMGIC 对牙本质的 SBS,可以考虑将这种材料更广泛地应用于临床。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e069/10582219/487007d54001/CRE2-9-851-g001.jpg

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