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微波烧结制备3D打印氮化硅生物陶瓷

Preparation of 3D printed silicon nitride bioceramics by microwave sintering.

作者信息

Zeng Xiaofeng, Sipaut Coswald Stephen, Ismail Noor Maizura, Liu Yuandong, Farm Yan Yan, Peng Bo, He Jiayu

机构信息

Faculty of Engineering, University Malaysia Sabah, 88400, Kota Kinabalu, Sabah, Malaysia.

Hengyang Kaixin Special Material Technology Co., Ltd., Hengyang, 421200, China.

出版信息

Sci Rep. 2024 Jul 9;14(1):15825. doi: 10.1038/s41598-024-66942-w.

DOI:10.1038/s41598-024-66942-w
PMID:38982185
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC11233628/
Abstract

Silicon nitride (SiN) is a bioceramic material with potential applications. Customization and high reliability are the foundation for the widespread application of SiN bioceramics. This study constructed a new microwave heating structure and successfully prepared 3D printed dense SiN materials, overcoming the adverse effects of a large amount of 3D printed organic forming agents on degreasing and sintering processes, further improving the comprehensive performance of SiN materials. Compared with control materials, the 3D printed SiN materials by microwave sintering have the best mechanical performance: bending strength is 928 MPa, fracture toughness is 9.61 MPa·m. Meanwhile, it has the best biocompatibility and antibacterial properties, and cells exhibit the best activity on the material surface. Research has shown that the excellent mechanical performance and biological activity of materials are mainly related to the high-quality degreasing, high cleanliness sintering environment, and high-quality liquid-phase sintering of materials in microwave environments.

摘要

氮化硅（SiN）是一种具有潜在应用价值的生物陶瓷材料。定制化和高可靠性是SiN生物陶瓷广泛应用的基础。本研究构建了一种新型微波加热结构，并成功制备出3D打印致密SiN材料，克服了大量3D打印有机成型剂对脱脂和烧结过程的不利影响，进一步提高了SiN材料的综合性能。与对照材料相比，微波烧结的3D打印SiN材料具有最佳的力学性能：弯曲强度为928MPa，断裂韧性为9.61MPa·m。同时，它具有最佳的生物相容性和抗菌性能，细胞在材料表面表现出最佳活性。研究表明，材料优异的力学性能和生物活性主要与微波环境下材料的高质量脱脂、高清洁度烧结环境以及高质量的液相烧结有关。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d283/11233628/16f90f3bc22d/41598_2024_66942_Fig8_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d283/11233628/bc22ec7680e6/41598_2024_66942_Fig1_HTML.jpg
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https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d283/11233628/2cacabcba917/41598_2024_66942_Fig5_HTML.jpg
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https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d283/11233628/5de75796e7e1/41598_2024_66942_Fig7_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d283/11233628/16f90f3bc22d/41598_2024_66942_Fig8_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d283/11233628/bc22ec7680e6/41598_2024_66942_Fig1_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d283/11233628/dd651556b6df/41598_2024_66942_Fig2_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d283/11233628/8a873e0fb78c/41598_2024_66942_Fig3_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d283/11233628/2121faa60e6f/41598_2024_66942_Fig4_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d283/11233628/2cacabcba917/41598_2024_66942_Fig5_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d283/11233628/cae66c5c5b90/41598_2024_66942_Fig6_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d283/11233628/5de75796e7e1/41598_2024_66942_Fig7_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d283/11233628/16f90f3bc22d/41598_2024_66942_Fig8_HTML.jpg

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