Harless R L, Harris D E, Sovocool G W, Zehr R D, Wilson N K, Oswald E O
Biomed Mass Spectrom. 1978 Mar;5(3):232-7. doi: 10.1002/bms.1200050312.
A specific portion of our environment has been contaminated with Kepone, or chlordecone. Additionally, some specific human exposures to high concentrations of Kepone have been confirmed. Gas chromatography mass spectrometry involving chemical ionization and high resolution mass spectrometry were used to detect, identify and confirm the presence of Kepone, Kepone photoproducts and a reduction product of Kepone in environmental and human samples. Field desorption, field ionization and electron impact mass spectrometric methods, as well as infrared and nuclear magnetic resonance techniques were used to characterize and identify Kepone hydrate and hemiketal in benzene and methanol solutions, respectively.
我们环境中的特定部分已被开蓬（即十氯酮）污染。此外，已证实存在一些人类接触高浓度开蓬的情况。采用涉及化学电离和高分辨率质谱的气相色谱 - 质谱联用技术，来检测、鉴定和确认环境及人体样本中开蓬、开蓬光产物以及开蓬还原产物的存在。分别运用场解吸、场电离和电子轰击质谱方法，以及红外和核磁共振技术，对苯和甲醇溶液中的开蓬水合物和半缩酮进行表征和鉴定。
