采用电化学阵列检测液相色谱法对商业产品中的姜成分进行定量分析。
Quantitative analysis of ginger components in commercial products using liquid chromatography with electrochemical array detection.
机构信息
Center for Excellence in Post-Harvest Technologies, North Carolina Agricultural and Technical State University, North Carolina Research Campus, 500 Laureate Way, Kannapolis, North Carolina 28081, United States.
出版信息
J Agric Food Chem. 2010 Dec 22;58(24):12608-14. doi: 10.1021/jf1029256. Epub 2010 Nov 23.
Abstract
For the first time, a sensitive reversed-phase HPLC electrochemical array method has been developed for the quantitative analysis of 8 major ginger components ([6]-, [8]-, and [10]-gingerol, [6]-, [8]-, and [10]-shogaol, [6]-paradol, and [1]-dehydrogingerdione) in 11 ginger-containing commercial products. This method was valid with unrivaled sensitivity as low as 7.3-20.2 pg of limit of detection and a range of 14.5-40.4 pg for the limit of quantification. The levels of 8 ginger components in 11 different commercial products were quantified by use of this method. The results found that both levels and ratios among the 8 compounds vary greatly in commercial products.
摘要
首次建立了一种灵敏的反相高效液相色谱电化学阵列法，用于定量分析 11 种含姜商业产品中的 8 种主要姜成分（[6]-、[8]-和[10]-姜醇、[6]-、[8]-和[10]-姜烯酚、[6]-对丙烯基酚和[1]-脱氢姜二酮）。该方法具有无与伦比的灵敏度，检测限低至 7.3-20.2pg，定量限范围为 14.5-40.4pg。使用该方法定量测定了 11 种不同商业产品中 8 种姜成分的含量。结果发现，商业产品中 8 种化合物的含量和比例差异很大。
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