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Dichlorido{2-[2-(piperidin-1-yl)ethyl-imino-meth-yl]phenolato}zinc(II) monohydrate.

作者信息

Zhang Dong-Fang, Zhou Mei-Huan, Yuan Chang-Ji

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2008 May 17;64(Pt 6):m825-6. doi: 10.1107/S1600536808014311.

DOI:10.1107/S1600536808014311
PMID:21202508
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2961511/
Abstract

In the title mononuclear zinc(II) complex, [ZnCl(2)(C(14)H(20)N(2)O)]·H(2)O, the Zn(II) atom is four-coordinated by the phenolate O and imine N atoms of the Schiff base ligand and by two Cl atoms in a tetra-hedral geometry. In the crystal structure, O-H⋯Cl, O-H⋯O and N-H⋯O hydrogen bonds involving the water mol-ecules bridge adjacent complexes into a ladder-like structure running along the c axis.

摘要
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/73b9/2961511/de8a5ae00b45/e-64-0m825-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/73b9/2961511/2a255cbf8fc9/e-64-0m825-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/73b9/2961511/de8a5ae00b45/e-64-0m825-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/73b9/2961511/2a255cbf8fc9/e-64-0m825-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/73b9/2961511/de8a5ae00b45/e-64-0m825-fig2.jpg

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Acta Crystallogr Sect E Struct Rep Online. 2008 Jun 7;64(Pt 7):m859-60. doi: 10.1107/S1600536808015730.

本文引用的文献

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Acta Crystallogr Sect E Struct Rep Online. 2008 Apr 26;64(Pt 5):m718-9. doi: 10.1107/S1600536808011161.
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Inorg Chem. 2008 Apr 21;47(8):3095-104. doi: 10.1021/ic7020758. Epub 2008 Mar 18.
3
A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.
4
Binuclear fluoro-bridged zinc and cadmium complexes of a schiff base expanded porphyrin: fluoride abstraction from the tetrafluoroborate anion.一种席夫碱扩展卟啉的双核氟桥联锌和镉配合物：从四氟硼酸根阴离子中夺取氟。
Inorg Chem. 2007 Aug 6;46(16):6224-6. doi: 10.1021/ic700933p. Epub 2007 Jul 14.