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不同采收期荆芥叶与穗中生物活性及有毒成分的定量比较分析。

Quantitative comparative analysis of the bio-active and toxic constituents of leaves and spikes of Schizonepeta tenuifolia at different harvesting times.

机构信息

Jiangsu Key Laboratory for High Technology Research of TCM Formulae, Nanjing University of Chinese Medicine, Nanjing 210046, China; E-Mails:

出版信息

Int J Mol Sci. 2011;12(10):6635-44. doi: 10.3390/ijms12106635. Epub 2011 Oct 10.

DOI:10.3390/ijms12106635
PMID:22072908
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC3210999/
Abstract

A GC-MS-Selected Ion Monitoring (SIM) detection method was developed for simultaneous determination of four monoterpenes: (-)-menthone, (+)-pulegone, (-)-limonene and (+)-menthofuran as the main bio-active and toxic constituents, and four other main compounds in the volatile oils of Schizonepeta tenuifolia (ST) leaves and spikes at different harvesting times. The results showed that the method was simple, sensitive and reproducible, and that harvesting time was a possible key factor in influencing the quality of ST leaves, but not its spikes. The research might be helpful for determining the harvesting time of ST samples and establishing a validated method for the quality control of ST volatile oil and other relative products.

摘要

建立了一种气相色谱-选择离子监测（SIM）检测方法，用于同时测定荆芥穗和荆芥挥发油中 4 种单萜类化合物：（-）-薄荷酮、（+）-胡椒酮、（-）-柠檬烯和（+）-薄荷呋喃（作为主要的生物活性和毒性成分），以及 4 种其他主要化合物。结果表明，该方法简单、灵敏、重现性好，收获时间可能是影响荆芥穗质量的关键因素，但对其荆芥的质量没有影响。本研究可能有助于确定荆芥样品的最佳采收期，并为荆芥挥发油及其他相关产品的质量控制建立一个有效的方法。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2b2e/3210999/4b69917fc515/ijms-12-06635f2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2b2e/3210999/ed91b9243920/ijms-12-06635f1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2b2e/3210999/4b69917fc515/ijms-12-06635f2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2b2e/3210999/ed91b9243920/ijms-12-06635f1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2b2e/3210999/4b69917fc515/ijms-12-06635f2.jpg

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