Chamard V, Allain M, Godard P, Talneau A, Patriarche G, Burghammer M
Aix-Marseille Université, CNRS, Centrale Marseille, Institut Fresnel UMR7249, 13013 Marseille, France.
1] Aix-Marseille Université, CNRS, Centrale Marseille, Institut Fresnel UMR7249, 13013 Marseille, France [2] Institut P' (UPR 3346 CNRS), Université de Poitiers, ENSMA, Bd Pierre et Marie Curie, 86962 Futuroscope, France.
Sci Rep. 2015 May 18;5:9827. doi: 10.1038/srep09827.
Progresses in the design of well-defined electronic band structure and dedicated functionalities rely on the high control of complex architectural device nano-scaled structures. This includes the challenging accurate description of strain fields in crystalline structures, which requires non invasive and three-dimensional (3D) imaging methods. Here, we demonstrate in details how x-ray Bragg ptychography can be used to quantify in 3D a displacement field in a lithographically patterned silicon-on-insulator structure. The image of the crystalline properties, which results from the phase retrieval of a coherent intensity data set, is obtained from a well-controlled optimized process, for which all steps are detailed. These results confirm the promising perspectives of 3D Bragg ptychography for the investigation of complex nano-structured crystals in material science.
在设计明确的电子能带结构和特定功能方面取得的进展依赖于对复杂架构器件纳米级结构的高度控制。这包括对晶体结构中应变场进行具有挑战性的精确描述,而这需要非侵入性的三维(3D)成像方法。在此,我们详细展示了如何使用X射线布拉格叠层成像术在三维空间中量化绝缘体上硅光刻图案化结构中的位移场。晶体特性图像是通过对相干强度数据集进行相位恢复得到的,它来自一个经过精心控制的优化过程,该过程的所有步骤都有详细说明。这些结果证实了三维布拉格叠层成像术在材料科学中研究复杂纳米结构晶体方面具有广阔的前景。