Nadaroglu Hayrunnisa, Onem Hicran, Alayli Gungor Azize
Department of Nano-Science and Nano-Engineering, Faculty of Engineering, Ataturk University, 25240 Erzurum, Turkey.
Department of Food Technology, Erzurum Vocational Training School, Ataturk University, 25240 Erzurum, Turkey.
IET Nanobiotechnol. 2017 Jun;11(4):411-419. doi: 10.1049/iet-nbt.2016.0138.
In this study, the authors presented synthesis of ceria nanoparticles (NPs) by the bio-reduction method and their antioxidative activity. Aqueous extract of () was used as reducing and stabilising agents. They used aqueous extract of () as reducing and stabilising agent. Ultraviolet-visible (UV-vis) absorption spectroscopy was used to monitor the quantitative formation of ceria NPs. They also addressed the characteristics of the obtained ceria NPs using scanning electron microscopy (SEM), X-ray diffraction (XRD) and transmitting electron microscope (TEM). The synthesised cerium (III) oxide (CeO) NPs were initially noted through visual colour change from colourless pale yellow cerium (III) to light yellow cerium (IV) and further confirmed the band at 345 nm employing UV-vis spectroscopy. The average diameter of the prepared NPs was about 8.6-10.5 nm. In addition, the synthesised CeO NPs were tested for antioxidant and anti-bacterial activities using ferric reducing antioxidant power, cupric reducing antioxidant capacity, ferrous ions chelating activity, superoxide the anion radical scavenging and 2, 2'-azinobis 3-ethylbenzothiazol to-6-sulphonic acid scavenging activity. It could be concluded that () extract can be used efficiently in the production of potential antioxidant and anti-bacterial CeO NPs for commercial applications.
在本研究中,作者介绍了通过生物还原法合成二氧化铈纳米颗粒(NPs)及其抗氧化活性。使用()的水提取物作为还原剂和稳定剂。他们使用()的水提取物作为还原剂和稳定剂。采用紫外-可见(UV-vis)吸收光谱法监测二氧化铈纳米颗粒的定量形成。他们还使用扫描电子显微镜(SEM)、X射线衍射(XRD)和透射电子显微镜(TEM)研究了所得二氧化铈纳米颗粒的特性。合成的氧化铈(CeO)纳米颗粒最初通过从无色浅黄色铈(III)到浅黄色铈(IV)的视觉颜色变化被注意到,并采用紫外-可见光谱法进一步确认了345 nm处的吸收带。制备的纳米颗粒的平均直径约为8.6-10.5 nm。此外,使用铁还原抗氧化能力、铜还原抗氧化能力、亚铁离子螯合活性、超氧阴离子自由基清除和2,2'-偶氮双(3-乙基苯并噻唑啉-6-磺酸)清除活性对合成的CeO纳米颗粒进行了抗氧化和抗菌活性测试。可以得出结论,()提取物可有效地用于生产具有潜在抗氧化和抗菌性能的CeO纳米颗粒,用于商业应用。