Suppr超能文献

经铬酸盐处理表面、钝化酸处理及氩等离子体去污后钛的表面特性

Superficial Characteristics of Titanium after Treatment of Chorreated Surface, Passive Acid, and Decontamination with Argon Plasma.

作者信息

Rizo-Gorrita María, Luna-Oliva Irene, Serrera-Figallo María-Angeles, Torres-Lagares Daniel

机构信息

Dental School, University of Sevilla, 41009 Seville, Spain.

出版信息

J Funct Biomater. 2018 Dec 11;9(4):71. doi: 10.3390/jfb9040071.

Abstract

(1) Background. Titanium is characterized by its biocompatibility, resistance to maximum stress, and fatigue and non-toxicity. The composition, surface structure, and roughness of titanium have a key and direct influence on the osseointegration processes when it is used in the form of dental implants. The objective of the present study is to characterize, at chemical, superficial, and biological levels, the result of the application of the sandblasted with large-grit and acid-etched (SLA) treatment consisting of coarse-grained and double-passivated acid blasting with subsequent decontamination with argon plasma on the surface of titanium implants type IV. (2) Methods. Four Oxtein dental implants (Zaragoza, Spain) were investigated with the following coding: Code L63713T (titanium grade IV, 3.75 mm in diameter, and 13 mm in length). The surface of the implants was SLA type obtained from coarse-grained, double passivated acid, and decontaminated with argon plasma. The samples were in their sealed packages and were opened in our laboratory. The X-ray photoelectron spectroscopy (XPS) technique was used to characterize the chemical composition of the surface, and the scanning electronic microscope (SEM) technique was used to perform topographic surface evaluation. Cell cultures were also performed on both surfaces. (3) Results. The superficial chemical analysis of the studied samples presented the following components, approximately, expressed in atomic percentage: O: 39%; Ti: 18%; C: 39%; N: 2%; and Si: 1%. In the same way, the topographic analysis values were obtained in the evaluated roughness parameters: R: 1.5 μm ± 0.02%; R: 1.31 μm ± 0.33; R: 8.98 μm ± 0.73; R: 5.12 μm ± 0.48; R: 3.76 μm ± 0.51; and R: 4.92 μm ± 0.24. At a biological level, the expression of osteocalcin was higher ( < 0.05) on the micro-rough surface compared to that machined at 48 and 96 h of culture. (4) Conclusions. The data obtained in our study indicate that the total carbon content, the relative concentration of titanium, and the roughness of the treatment performed on the implants are in agreement with those found in the literature. Further, the roughness of the treatment performed on the implants throws a spongy, three-dimensional surface suitable for bone growth on it. The biological results found are compatible with the clinical use of the surface tested.

摘要

(1) 背景。钛具有生物相容性、抗最大应力性、抗疲劳性以及无毒的特性。当钛以牙种植体的形式使用时,其成分、表面结构和粗糙度对骨结合过程具有关键且直接的影响。本研究的目的是在化学、表面和生物学层面上,对采用大颗粒喷砂和酸蚀(SLA)处理(包括粗颗粒和双钝化酸喷砂,随后用氩等离子体进行表面净化)应用于IV型钛种植体表面的结果进行表征。(2) 方法。对四个Oxtein牙种植体(西班牙萨拉戈萨)进行了研究,其编码如下:编码L63713T(IV级钛,直径3.75毫米,长度13毫米)。种植体表面为SLA型,通过粗颗粒、双钝化酸处理获得,并经氩等离子体净化。样本处于密封包装中,在我们的实验室中打开。使用X射线光电子能谱(XPS)技术对表面化学成分进行表征,使用扫描电子显微镜(SEM)技术进行表面形貌评估。还在两个表面上进行了细胞培养。(3) 结果。对所研究样本的表面化学分析呈现出以下成分,大致以原子百分比表示:O:39%;Ti:18%;C:39%;N:2%;Si:1%。同样,在评估的粗糙度参数中获得了形貌分析值:R:1.5μm±0.02%;R:1.31μm±0.33;R:8.98μm±0.73;R:5.12μm±0.48;R:3.76μm±0.51;R:4.92μm±0.24。在生物学层面上,与培养48小时和96小时时的机械加工表面相比,微粗糙表面上骨钙素的表达更高(<0.05)。(4) 结论。我们研究中获得的数据表明,种植体上处理后的总碳含量、钛的相对浓度以及粗糙度与文献中发现的一致。此外,种植体上处理后的粗糙度形成了一个适合骨生长的海绵状三维表面。所发现的生物学结果与测试表面的临床应用相符。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d39a/6306932/f72b48e54cbc/jfb-09-00071-g001.jpg

文献检索

告别复杂PubMed语法,用中文像聊天一样搜索,搜遍4000万医学文献。AI智能推荐,让科研检索更轻松。

立即免费搜索

文件翻译

保留排版,准确专业,支持PDF/Word/PPT等文件格式,支持 12+语言互译。

免费翻译文档

深度研究

AI帮你快速写综述,25分钟生成高质量综述,智能提取关键信息,辅助科研写作。

立即免费体验