Moradi Mona, Azizi-Lalabadi Maryam, Motamedi Parisa, Sadeghi Ehsan
Department of Chemical Engineering- Food Sciences Kermanshah Science and Research Branch Islamic Azad University Kermanshah Iran.
Research Center for Environmental Determinants of Health (RCEDH) Kermanshah University of Medical Sciences Kermanshah Iran.
Food Sci Nutr. 2021 Jan 8;9(2):1171-1179. doi: 10.1002/fsn3.2097. eCollection 2021 Feb.
Fabricating graphite electrode corrected with nanofiber by electrospinning as a considerable procedure for utilization in the fluid materials, milk, and syrup for detection of T mycotoxin is a significant technique. The modern biosensor was fabricated at normal degrees of room and utilized via buffer Britton-Robinson (B-R) in pH = 5 to refine the chemico-mechanical specifications. The electrochemical manner of the modified surface was surveyed using the scanning electron microscopy (SEM), cyclic voltammetry (CV), square wave voltammetry (SQWV), electrochemical impedance spectroscopy (EIS), and differential pulse voltammetry (DPV). The corrected electrode displayed a linear reply to T toxin in two distinct concentration ranges of 30-100 nM with correlation coefficients of 0.99. The greatest signals in the square wave spectrums for the B-R buffer created on the uttermost signals of the obtained streams were pH = 5 and 0.5 M of KNO for T toxin. The modified electrode has a big signal, broad dynamic concentration and high sensitivity and selectivity.
通过静电纺丝制备用纳米纤维校正的石墨电极作为用于流体材料、牛奶和糖浆中检测T型霉菌毒素的一种重要方法是一项重要技术。现代生物传感器在正常室温下制造,并通过pH = 5的缓冲布里顿-罗宾逊(B-R)溶液使用,以改善化学机械性能。使用扫描电子显微镜(SEM)、循环伏安法(CV)、方波伏安法(SQWV)、电化学阻抗谱(EIS)和差分脉冲伏安法(DPV)研究了修饰表面的电化学行为。校正后的电极在30-100 nM的两个不同浓度范围内对T毒素呈现线性响应,相关系数为0.99。对于在所得电流的最大信号上产生的B-R缓冲液,方波谱中的最大信号是pH = 5和0.5 M的KNO用于T毒素。修饰电极具有大信号、宽动态浓度范围以及高灵敏度和选择性。