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I22:英国钻石光源同步辐射小角散射和广角散射光束线站——十年运行概述。

I22: SAXS/WAXS beamline at Diamond Light Source - an overview of 10 years operation.

机构信息

Diamond Light Source Ltd, Diamond House, Harwell Science and Innovation Campus, Didcot, Oxfordshire OX11 0DE, United Kingdom.

King's College London, Guy's Campus, Great Maze Pond, London SE1 1UL, United Kingdom.

出版信息

J Synchrotron Radiat. 2021 May 1;28(Pt 3):939-947. doi: 10.1107/S1600577521002113. Epub 2021 Mar 15.

Abstract

Beamline I22 at Diamond Light Source is dedicated to the study of soft-matter systems from both biological and materials science. The beamline can operate in the range 3.7 keV to 22 keV for transmission SAXS and 14 keV to 20 keV for microfocus SAXS with beam sizes of 240 µm × 60 µm [full width half-maximum (FWHM) horizontal (H) × vertical (V)] at the sample for the main beamline, and approximately 10 µm × 10 µm for the dedicated microfocusing platform. There is a versatile sample platform for accommodating a range of facilities and user-developed sample environments. The high brilliance of the insertion device source on I22 allows structural investigation of materials under extreme environments (for example, fluid flow at high pressures and temperatures). I22 provides reliable access to millisecond data acquisition timescales, essential to understanding kinetic processes such as protein folding or structural evolution in polymers and colloids.

摘要

英国钻石光源的 I22 光束线专门用于研究生物和材料科学领域的软物质体系。该光束线的工作范围为 3.7keV 至 22keV,适用于透射小角 X 射线散射(SAXS),14keV 至 20keV 适用于微聚焦 SAXS,在主光束线上,水平(H)和垂直(V)方向的光束尺寸为 240μm×60μm(全宽半最大值),专用微聚焦平台的光束尺寸约为 10μm×10μm。该光束线有一个多功能的样品平台,可容纳各种设备和用户开发的样品环境。I22 上的插入器件光源具有很高的亮度,可在极端环境下(例如,高压高温下的流体流动)对材料进行结构研究。I22 提供了可靠的访问毫秒级数据采集时间尺度的途径,这对于理解蛋白质折叠或聚合物和胶体中的结构演化等动力学过程至关重要。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/25ff/8127364/dfa31dc7fdb2/s-28-00939-fig1.jpg

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