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通过壳聚糖纳米颗粒增强纤维素织物的抗菌和染色性能

Enhancement of Antimicrobial and Dyeing Properties of Cellulosic Fabrics via Chitosan Nanoparticles.

作者信息

Mosaad Rehab M, Alhalafi Mona H, Emam El-Amir M, Ibrahim Marwan A, Ibrahim Hassan

机构信息

Department of Biology, College of Science, Majmaah University, AL-Majmaah 11952, Saudi Arabia.

Faculty of Women for Arts, Science and Education, Ain Shams University, Cairo 11566, Egypt.

出版信息

Polymers (Basel). 2022 Oct 7;14(19):4211. doi: 10.3390/polym14194211.

Abstract

The primary goal of this study is to prepare chitosan nanoparticles (CSNPs) by the ionic gelation method via the treatment of chitosan (0.2 wt.%) with tripolyphosphate (0.2 wt.%) ultrasonically for 45 min. FT-IR spectroscopy and TEM images were used to characterize and validate CSNP production. Cellulosic materials with different concentrations of CSNPs have better antibacterial and colouring characteristics. The treated cellulosic fabrics were analyzed by FT-IR spectroscopy, SEM, and thermogravimetric analysis. Colourimetric data measurements expressed in K/S values were used to evaluate the impact of CSNPs on the dyeing affinity of cellulosic materials. In addition, antibacterial activity against bacteria and fungi was tested on the treated cellulosic fabrics. According to the K/S values, cellulosic textiles treated with CSNPs (0.3 wt.%) had a better affinity for acid dyeing. These textiles also offer better antibacterial properties and are more resistant to washing, light, and rubbing. A cytotoxicity study found that CSNPs give cellulosic materials antibacterial and acid dyeing properties, which is good for the environment.

摘要

本研究的主要目标是通过离子凝胶法,用三聚磷酸钠(0.2 wt.%)对壳聚糖(0.2 wt.%)进行超声处理45分钟来制备壳聚糖纳米颗粒(CSNPs)。采用傅里叶变换红外光谱(FT-IR)和透射电子显微镜(TEM)图像对CSNP的制备进行表征和验证。含有不同浓度CSNPs的纤维素材料具有更好的抗菌和染色特性。通过FT-IR光谱、扫描电子显微镜(SEM)和热重分析对处理后的纤维素织物进行分析。用K/S值表示的比色数据测量用于评估CSNPs对纤维素材料染色亲和力的影响。此外,还对处理后的纤维素织物进行了针对细菌和真菌的抗菌活性测试。根据K/S值,用CSNPs(0.3 wt.%)处理的纤维素纺织品对酸性染色具有更好的亲和力。这些纺织品还具有更好的抗菌性能,并且更耐洗涤、光照和摩擦。细胞毒性研究发现,CSNPs赋予纤维素材料抗菌和酸性染色性能,这对环境有益。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/cef7/9573385/eb71e39c4a90/polymers-14-04211-g001.jpg

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