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微波辅助合成螺杂环化合物的研究进展

Recent advances in microwave-assisted multicomponent synthesis of spiro heterocycles.

作者信息

Javahershenas Ramin, Makarem Ata, Klika Karel D

机构信息

Department of Organic Chemistry, Faculty of Chemistry, Urmia University Urmia Iran

Institute of Pharmacy, University of Hamburg 20146 Hamburg Germany.

出版信息

RSC Adv. 2024 Feb 13;14(8):5547-5565. doi: 10.1039/d4ra00056k. eCollection 2024 Feb 7.

DOI:10.1039/d4ra00056k
PMID:38357035
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC10866134/
Abstract

Spiro heterocycle frameworks are a class of organic compounds that possesses unique structural features making them highly sought-after targets in drug discovery due to their diverse biological and pharmacological activities. Microwave-assisted organic synthesis has emerged as a powerful tool for assembling complex molecular architectures. The use of microwave irradiation in synthetic chemistry is a promising method for accelerating reaction rates and improving yields. This review provides insights into the current state of the art and highlights the potential of microwave-assisted multicomponent reactions in the synthesis of novel spiro heterocyclic compounds that were reported between 2017 and 2023.

摘要

螺杂环骨架是一类有机化合物，因其多样的生物和药理活性而具有独特的结构特征，使其成为药物发现中备受追捧的目标。微波辅助有机合成已成为组装复杂分子结构的有力工具。在合成化学中使用微波辐射是加速反应速率和提高产率的一种有前景的方法。本综述深入探讨了当前的技术现状，并突出了2017年至2023年间报道的微波辅助多组分反应在新型螺杂环化合物合成中的潜力。

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Chem Rev. 2024 Mar 13;124(5):2651-2698. doi: 10.1021/acs.chemrev.3c00794. Epub 2023 Dec 29.
5
Recent developments on microwave-assisted organic synthesis of nitrogen- and oxygen-containing preferred heterocyclic scaffolds.微波辅助有机合成含氮和含氧优势杂环骨架的最新进展。
RSC Adv. 2023 Nov 7;13(47):32858-32892. doi: 10.1039/d3ra05986c.
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Chemo-/Regio-Selective Synthesis of Novel Functionalized Spiro[pyrrolidine-2,3'-oxindoles] under Microwave Irradiation and Their Anticancer Activity.微波辐射下新型功能化螺[吡咯烷-2,3'-氧吲哚]的 chemo-/Regio-选择性合成及其抗癌活性。
Molecules. 2023 Sep 7;28(18):6503. doi: 10.3390/molecules28186503.
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Natural-Product-Inspired Microwave-Assisted Synthesis of Novel Spirooxindoles as Antileishmanial Agents: Synthesis, Stereochemical Assignment, Bioevaluation, SAR, and Molecular Docking Studies.受天然产物启发的微波辅助新型螺环氧化吲哚类抗利什曼原虫剂的合成：合成、立体化学归属、生物评价、SAR 和分子对接研究。
Molecules. 2023 Jun 16;28(12):4817. doi: 10.3390/molecules28124817.
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Microwave produced 8-methyl-1,2,4,8-tetraazaspiro[4.5]dec-2-en-3-amine derivatives: their in vitro and in silico analysis.微波合成 8-甲基-1,2,4,8-四氮杂螺[4.5]癸-2-烯-3-胺衍生物：体外和计算分析。
Mol Divers. 2024 Jun;28(3):1409-1422. doi: 10.1007/s11030-023-10665-z. Epub 2023 Jun 6.
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Recent advances in the multicomponent synthesis of heterocycles using tetronic acid.利用特窗酸进行杂环化合物多组分合成的最新进展。
RSC Adv. 2023 Jun 2;13(24):16619-16629. doi: 10.1039/d3ra02505e. eCollection 2023 May 30.
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Recent Studies on the Application of Microwave-Assisted Method for the Preparation of Heterogeneous Catalysts and Catalytic Hydrogenation Processes.近期关于微波辅助法在制备多相催化剂和催化加氢过程中应用的研究。
Int J Mol Sci. 2023 May 5;24(9):8272. doi: 10.3390/ijms24098272.