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钛合金基底上的双层溶胶-凝胶改性——物理化学性质评估

Double-Layer Sol-Gel Modifications on Titanium Alloy Substrates-Physicochemical Properties Evaluation.

作者信息

Matysiak Katarzyna, Biegun-Żurowska Maria, Cholewa-Kowalska Katarzyna, Goryczka Tomasz, Zając Wojciech, Ziąbka Magdalena

机构信息

Department of Ceramics and Refractories, Faculty of Materials Science and Ceramics, AGH University of Krakow, 30-059 Krakow, Poland.

Department of Glass Technology and Amorphous Coatings, Faculty of Materials Science and Ceramics, AGH University of Krakow, 30-059 Krakow, Poland.

出版信息

Materials (Basel). 2025 Aug 18;18(16):3857. doi: 10.3390/ma18163857.

DOI:10.3390/ma18163857
PMID:40870176
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC12387934/
Abstract

The objective of this study was to investigate the physicochemical properties of hybrid coatings with titanium nitride and boron nitride nanoparticles deposited on the TiAlV medical alloy via the sol-gel process. The developed layers were intended to impart bactericidal properties and provide protection against surgical abrasions during the implantation procedure. This study focused on evaluating the microstructure (SEM + EDS), structure (XRD, FTIR), and surface properties, including wettability, surface free energy, and roughness of the synthesized layers. Our results confirmed that it was feasible to produce hybrid layers with various microstructures and diverse layer morphologies. The FTIR and XRD structural analyses confirmed the presence of an organosilicon matrix incorporating the two aforementioned types of ceramic particles.

摘要

本研究的目的是通过溶胶-凝胶工艺研究沉积在TiAlV医用合金上的氮化钛和氮化硼纳米颗粒混合涂层的物理化学性质。所制备的涂层旨在赋予杀菌性能，并在植入过程中提供抗手术磨损的保护。本研究着重评估合成涂层的微观结构（扫描电子显微镜+能谱仪）、结构（X射线衍射仪、傅里叶变换红外光谱仪）以及表面性质，包括润湿性、表面自由能和粗糙度。我们的结果证实，制备具有各种微观结构和不同层形态的混合涂层是可行的。傅里叶变换红外光谱仪和X射线衍射仪的结构分析证实了含有上述两种陶瓷颗粒的有机硅基体的存在。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/15e3/12387934/0934f502686a/materials-18-03857-g012.jpg
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https://cdn.ncbi.nlm.nih.gov/pmc/blobs/15e3/12387934/cebca8d15748/materials-18-03857-g005.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/15e3/12387934/413c4e1742db/materials-18-03857-g006.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/15e3/12387934/faa5aca3ef63/materials-18-03857-g007.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/15e3/12387934/34d22fd63a66/materials-18-03857-g008.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/15e3/12387934/7aebaff89380/materials-18-03857-g009.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/15e3/12387934/f2266774d445/materials-18-03857-g010.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/15e3/12387934/f21c28e37b06/materials-18-03857-g011.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/15e3/12387934/0934f502686a/materials-18-03857-g012.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/15e3/12387934/8583c30da6f8/materials-18-03857-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/15e3/12387934/68fc66311b83/materials-18-03857-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/15e3/12387934/0c184203c9ab/materials-18-03857-g003.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/15e3/12387934/d7d9bdbc7af4/materials-18-03857-g004.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/15e3/12387934/cebca8d15748/materials-18-03857-g005.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/15e3/12387934/413c4e1742db/materials-18-03857-g006.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/15e3/12387934/faa5aca3ef63/materials-18-03857-g007.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/15e3/12387934/34d22fd63a66/materials-18-03857-g008.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/15e3/12387934/7aebaff89380/materials-18-03857-g009.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/15e3/12387934/f2266774d445/materials-18-03857-g010.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/15e3/12387934/f21c28e37b06/materials-18-03857-g011.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/15e3/12387934/0934f502686a/materials-18-03857-g012.jpg

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本文引用的文献

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Research Progress of Titanium-Based Alloys for Medical Devices.医用钛基合金的研究进展
Biomedicines. 2023 Nov 8;11(11):2997. doi: 10.3390/biomedicines11112997.
3
Corrosion Behavior of Nitrided Layer of Ti6Al4V Titanium Alloy by Hollow Cathodic Plasma Source Nitriding.空心阴极等离子体源渗氮Ti6Al4V钛合金渗氮层的腐蚀行为
Materials (Basel). 2023 Apr 7;16(8):2961. doi: 10.3390/ma16082961.
4
Quantification of hexagonal boron nitride impurities in boron nitride nanotubes FTIR spectroscopy.氮化硼纳米管中六方氮化硼杂质的定量分析：傅里叶变换红外光谱法
Nanoscale Adv. 2019 Mar 12;1(5):1693-1701. doi: 10.1039/c8na00251g. eCollection 2019 May 15.
5
Antibacterial effect of boron nitride flakes with controlled orientation in polymer composites.聚合物复合材料中具有可控取向的氮化硼薄片的抗菌效果。
RSC Adv. 2019 Oct 17;9(57):33454-33459. doi: 10.1039/c9ra06773f. eCollection 2019 Oct 15.
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Selective modification of Ti6Al4V surfaces for biomedical applications.用于生物医学应用的Ti6Al4V表面的选择性改性。
RSC Adv. 2020 May 6;10(30):17642-17652. doi: 10.1039/c9ra11000c. eCollection 2020 May 5.
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Materials (Basel). 2021 Oct 21;14(21):6249. doi: 10.3390/ma14216249.
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