Roussi V, Govaris A, Varagouli A, Botsoglou N A
Institute of Biochemistry, Toxicology and Nourishment of Animals, Ministry of Agriculture, Athens, Greece.
Food Addit Contam. 2002 Sep;19(9):863-8. doi: 10.1080/02652030210146864.
From December 1999 to May 2000, 114 samples of pasteurized, ultrahigh temperature-treated (UHT) and concentrated milk were collected in supermarkets, whereas 52 raw milk samples from cow, sheep and goat were obtained from different milk producers all over Greece. Sample collection was repeated from December 2000 to May 2001 and concerned 54 samples of pasteurized milk, 23 samples of bulk-tank raw milk and 55 raw milk samples from cow, sheep and goat. The total number of samples analysed for aflatoxin M(1) (AFM(1)) contamination by immunoaffinity column extraction and liquid chromatography was 297. In the first sampling, the incidence rates of AFM(1) contamination in pasteurized, UHT, concentrated and cow, sheep and goat raw milk were 85.4, 82.3, 93.3, 73.3, 66.7 and 40%, respectively, with only one cow raw milk and two concentrated milk samples exceeding the EU limit of 50 ng l(-1). In the second sampling, the incidence rates of AFM(1) contamination in pasteurized, bulk-tank and cow, sheep and goat raw milk were 79.6, 78.3, 64.3, 73.3 and 66.7%, respectively, with only one cow and one sheep raw milk samples exceeding the limit of 50 ng l(-1). The results suggest that the current regulatory status in Greece is effective.
1999年12月至2000年5月，在超市采集了114份巴氏杀菌奶、超高温处理（UHT）奶和浓缩奶样本，同时从希腊各地不同的牛奶生产商处获取了52份牛、羊、山羊的生奶样本。2000年12月至2001年5月重复进行了样本采集，涉及54份巴氏杀菌奶样本、23份大容量储存生奶样本以及55份牛、羊、山羊的生奶样本。通过免疫亲和柱萃取和液相色谱法分析黄曲霉毒素M(1)（AFM(1)）污染情况的样本总数为297份。在首次采样中，巴氏杀菌奶、UHT奶、浓缩奶以及牛、羊、山羊生奶中AFM(1)污染的发生率分别为85.4%、82.3%、93.3%、73.3%、66.7%和40%，只有1份牛生奶样本和2份浓缩奶样本超过了欧盟50 ng l(-1)的限量标准。在第二次采样中，巴氏杀菌奶、大容量储存生奶以及牛、羊、山羊生奶中AFM(1)污染的发生率分别为79.6%、78.3%、64.3%、73.3%和66.7%，只有1份牛生奶样本和1份羊生奶样本超过了50 ng l(-1)的限量标准。结果表明希腊目前的监管状况是有效的。
