Jung Ui-Won, Hwang Ji-Wan, Choi Da-Yae, Hu Kyung-Seok, Kwon Mi-Kyung, Choi Seong-Ho, Kim Hee-Jin
Department of Periodontology, Research Institute for Periodontal Regeneration, Yonsei University College of Dentistry, Seoul, Korea.
J Periodontal Implant Sci. 2012 Apr;42(2):59-63. doi: 10.5051/jpis.2012.42.2.59. Epub 2012 Apr 30.
This study evaluated the surface characteristics and bond strength produced using a novel technique for coating hydroxyapatite (HA) onto titanium implants.
HA was coated on the titanium implant surface using a super-high-speed (SHS) blasting method with highly purified HA. The coating was performed at a low temperature, unlike conventional HA coating methods. Coating thickness was measured. The novel HA-coated disc was fabricated. X-ray diffraction analysis was performed directly on the disc to evaluate crystallinity. Four novel HA-coated discs and four resorbable blast medium (RBM) discs were prepared. Their surface roughnesses and areas were measured. Five puretitanium, RBM-treated, and novel HA-coated discs were prepared. Contact angle was measured. Two-way analysis of variance and the post-hoc Scheffe's test were used to analyze differences between the groups, with those with a probability of P<0.05 considered to be statistically significant. To evaluate exfoliation of the coating layer, 7 sites on the mandibles from 7 mongrel dogs were used. Other sites were used for another research project. In total, seven novel HA-coated implants were placed 2 months after extraction of premolars according to the manufacturer's instructions. The dogs were sacrificed 8 weeks after implant surgery. Implants were removed using a ratchet driver. The surface of the retrieved implants was evaluated microscopically.
A uniform HA coating layer was formed on the titanium implants with no deformation of the RBM titanium surface microtexture when an SHS blasting method was used.
These HA-coated implants exhibited increased roughness, crystallinity, and wettability when compared with RBM implants.
本研究评估了一种将羟基磷灰石(HA)涂覆于钛植入物上的新技术所产生的表面特性和结合强度。
使用超高速(SHS)喷砂法将高纯度HA涂覆在钛植入物表面。与传统的HA涂覆方法不同,该涂覆在低温下进行。测量涂层厚度。制作新型HA涂层圆盘。直接对圆盘进行X射线衍射分析以评估结晶度。制备了四个新型HA涂层圆盘和四个可吸收喷砂介质(RBM)圆盘。测量它们的表面粗糙度和面积。制备了五个纯钛、RBM处理和新型HA涂层圆盘。测量接触角。使用双向方差分析和事后Scheffe检验分析组间差异,P<0.05被认为具有统计学意义。为评估涂层的剥落情况,使用了7只杂种犬下颌骨上的7个部位。其他部位用于另一个研究项目。总共按照制造商的说明在拔除前磨牙2个月后植入了七个新型HA涂层植入物。在植入手术后8周处死犬只。使用棘轮螺丝刀取出植入物。对取出的植入物表面进行显微镜评估。
当使用SHS喷砂法时,在钛植入物上形成了均匀的HA涂层,RBM钛表面微观纹理未变形。
与RBM植入物相比,这些HA涂层植入物的粗糙度、结晶度和润湿性增加。