Yang Song-Yi, Kim Seong-Hwan, Choi Se-Young, Kim Kwang-Mahn
Department and Research Institute of Dental Biomaterials and Bioengineering, Yonsei University College of Dentistry, Seoul 03722, Korea.
BK21 PLUS Project, Yonsei University College of Dentistry, Seoul 03722, Korea.
Materials (Basel). 2016 Feb 24;9(3):125. doi: 10.3390/ma9030125.
The objective of the study was to compare the acid neutralizing ability and shear bond strength (SBS) of three different types of orthodontic adhesives containing bioactive glasses (BAGs). 45S5, 45S5F and S53P4 BAGs were prepared using the melting technique and ground to fine particles. Orthodontic adhesives containing three types of BAGs were prepared as follows: 52.5% 45S5 BAG + 17.5% glass (45S5_A); 61.25% 45S5 BAG + 8.75% glass (45S5_B); 52.5% 45S5F BAG + 17.5% glass (45S5F_A); 61.25% 45S5F BAG + 8.75% glass (45S5F_B); 52.5% S53P4 BAG + 17.5% glass (S53P4_A); 61.25% S53P4 BAG + 8.75% glass (S53P4_B); and 70.0% glass (BAG_0). To evaluate the acid neutralizing properties, specimens were immersed in lactic acid solution, and pH changes were measured. SBS was measured with a universal testing machine. For all of the BAG-containing adhesives, the one with 61.25% of BAG showed a significantly greater increase of pH than the one with 52.5% of BAG ( < 0.05). Groups with 61.25% of BAG showed lower SBS than samples with 52.5% of BAG. 45S5F_A showed no significant difference of SBS compared to BAG_0 ( > 0.05). The adhesive containing 61.25% of 45S5F BAG exhibited clinically acceptable SBS and acid neutralizing properties. Therefore, this composition is a suitable candidate to prevent white spot lesions during orthodontic treatment.
本研究的目的是比较三种不同类型含生物活性玻璃(BAGs)的正畸粘合剂的酸中和能力和剪切粘结强度(SBS)。采用熔融技术制备45S5、45S5F和S53P4 BAGs,并研磨成细颗粒。含三种类型BAGs的正畸粘合剂制备如下:52.5% 45S5 BAG + 17.5%玻璃(45S5_A);61.25% 45S5 BAG + 8.75%玻璃(45S5_B);52.5% 45S5F BAG + 17.5%玻璃(45S5F_A);61.25% 45S5F BAG + 8.75%玻璃(45S5F_B);52.5% S53P4 BAG + 17.5%玻璃(S53P4_A);61.25% S53P4 BAG + 8.75%玻璃(S53P4_B);以及70.0%玻璃(BAG_0)。为评估酸中和性能,将标本浸入乳酸溶液中,并测量pH值变化。用万能试验机测量SBS。对于所有含BAG的粘合剂,含61.25%BAG的粘合剂的pH值升高明显大于含52.5%BAG的粘合剂(<0.05)。含61.25%BAG的组的SBS低于含52.5%BAG的样品。45S5F_A与BAG_0相比,SBS无显著差异(>0.05)。含61.25% 45S5F BAG的粘合剂表现出临床上可接受的SBS和酸中和性能。因此,该组合物是正畸治疗期间预防白斑病变的合适候选物。