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利用叶提取物生物合成氧化铜纳米颗粒

Biosynthesis of copper oxide nanoparticles using leaf extract.

作者信息

Chand Mali Suresh, Raj Shani, Trivedi Rohini

机构信息

Department of Botany, Mohanlal Sukhadia University, Udaipur, 313001, Rajasthan, India.

出版信息

Biochem Biophys Rep. 2019 Nov 3;20:100699. doi: 10.1016/j.bbrep.2019.100699. eCollection 2019 Dec.

Abstract

In the present study copper oxide nanoparticles (CuONPs) were synthesized via simple and eco-friendly green route using leaf extract of (Lam.). Characterization of synthesized nanoparticles (NPs) was undertaken. The characteristic absorption peak of CuONPs was in range 264nm in UV-Vis spectrum. Scanning electron microscopy (SEM) and transmission electron microscopy (TEM) studies revealed the morphological and structural character of green NPs. The mean particle size was calculated to 30nm. Energy dispersive spectroscopy (EDS) showed high intense metallic peak of copper (Cu), oxygen (O) and low intense peaks of carbon (C), sulfur (S), phosphorus (P) elements due to the capping action of biomolecules of plant extract in CuONPs formation. The X-ray diffraction (XRD) pattern showed distinctive peaks corresponding to (200), (211) and (310) planes revealing the high crystalline nature of synthesized CuONPs with a primitive phase. Zeta potential and size distribution of synthesized green NPs was concluded by Dynamic light scattering (DLS) studies.

摘要

在本研究中,使用(某植物学名,此处原文未完整给出)的叶提取物通过简单且环保的绿色路线合成了氧化铜纳米颗粒(CuONPs)。对合成的纳米颗粒(NPs)进行了表征。CuONPs在紫外可见光谱中的特征吸收峰在264nm范围内。扫描电子显微镜(SEM)和透射电子显微镜(TEM)研究揭示了绿色纳米颗粒的形态和结构特征。计算得出平均粒径为30nm。能量色散光谱(EDS)显示,由于植物提取物的生物分子在CuONPs形成过程中的封端作用,铜(Cu)、氧(O)的金属峰强度较高,而碳(C)、硫(S)、磷(P)元素的峰强度较低。X射线衍射(XRD)图谱显示出对应于(200)、(211)和(310)晶面的独特峰,揭示了合成的CuONPs具有原始相的高结晶性质。通过动态光散射(DLS)研究得出了合成的绿色纳米颗粒的zeta电位和尺寸分布。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e243/6838746/2ecee57fb4a0/gr1.jpg

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